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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
24 December 2015 to 22 March 2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Guideline study under GLP, based on the results only a range could be defined
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7200 (Melting Point / Melting Range)
GLP compliance:
yes
Type of method:
other: differential scanning calorimetry
Key result
Decomposition:
yes
Decomp. temp.:
> 225 °C
Remarks on result:
other: at atmospheric pressure
Remarks:
the melting point could not deteremined due to evaporation and decomposition of the components

pre-test: decomposition (reduction of weight by 25% at 352 °C)

exp 1: glass transition between -58.17°C ; melting at 52.24°C (additional endothemic peak at ca 90 °C) 

exp 2:

first cycle: glass transition at -58.22 °C ; melting at 52.38°C (additional endothermic peak at 85 °C) 

second cycle: glass transition at -24.93 °C ; melting at 75.35°C ( no additional exothermic peak seen) 

 

 

Conclusions:
The melting temperature of the substance could not be determined
Executive summary:

Using the differential scanning calorimetric method the melting point of the substance could not deteremined due to evaporation and decomposition of the components

Description of key information

Using the differential scanning calorimetric method the melting point could not be determined due to evaporation and decomposition of the components

Key value for chemical safety assessment

Additional information