Registration Dossier
Registration Dossier
Use of this information is subject to copyright laws and may require the permission of the owner of the information, as described in the ECHA Legal Notice.
EC number: 947-917-0 | CAS number: -
Boiling point
Administrative data
Link to relevant study record(s)
- Endpoint:
- boiling point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 103 (Boiling Point)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.2 (Boiling Temperature)
- Version / remarks:
- 2008
- Deviations:
- no
- GLP compliance:
- no
- Type of method:
- differential scanning calorimetry
- Atm. press.:
- 1 020 hPa
- Decomposition:
- yes
- Decomp. temp.:
- >= 190 °C
- Remarks on result:
- not determinable
- Conclusions:
- Reaction product of lauryl-PDA/lauryl-DETA with chloroacetic acid does not have a boiling point until disintegration at about 190 °C.
- Executive summary:
The boiling temperature of Reaction product of lauryl-PDA/lauryl-DETA with chloroacetic acid was determined by thermogravimetry and differential scanning calorimetry according to the OECD Test Guideline 103 [adopted on 27 July 1995] and EU test method A.2.
No boiling point could be detected; decomposition started above 190 °C (1020 hPa).
Reference
The recorded main weight loss above 252.1 °C (estimated onset on TGA) may indicate a beginning evaporation (boiling). However, based on the visual inspection and the results of the DSC preliminary test (up to 250°C) a product decomposition is more likely.
In order to provide evidence for this assumption, a degradation test was performed during which an aliquot of the sample was heated to 190 °C for 15 minutes. The remaining residue (98 % of the original material) war characterised by NMR spectroscopy. The NMR analysis confirms the decomposition of the product. A significant loss of carbonyl functions was detected.
Consequently, the test item does not provide a boiling point until disintegration at about 190 °C.
Description of key information
decomposition before boiling
Key value for chemical safety assessment
Additional information
The boiling temperature of Reaction product of lauryl-PDA/lauryl-DETA with chloroacetic acid was determined by thermogravimetry and differential scanning calorimetry according to the OECD Test Guideline 103 [adopted on 27 July 1995] and EU test method A.2.
No boiling point could be detected; decomposition started above 190 °C (1020 hPa).
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
Reproduction or further distribution of this information may be subject to copyright protection. Use of the information without obtaining the permission from the owner(s) of the respective information might violate the rights of the owner.
