Registration Dossier

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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2015
Report date:
2015

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
no
Type of method:
thermal analysis
Remarks:
Differential Scanning Calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
(diethylamino)acetonitrile
EC Number:
221-130-6
EC Name:
(diethylamino)acetonitrile
Cas Number:
3010-02-4
Molecular formula:
C6H12N2
IUPAC Name:
2-(diethylamino)acetonitrile
Details on test material:
- Name of test material (as cited in study report): (Diethylamino)acetonitril
- Analytical purity: > 90%
- Lot/batch No.: Kwg. 7369593-3

Results and discussion

Melting / freezing point
Melting / freezing pt.:
-6 °C
Atm. press.:
1 013 hPa

Any other information on results incl. tables

The melting temperature of the test item was found at -6 °C peak temperature in the 2nd heating.

Determination  Onset temperature
[°C] 
Peak temperature
[°C] 
A -14.4 -6.1
B -14.2 -6.0
Mean value  -14 -6

The estimated accuracy is ± 1 °C.

The test item shows a glass transition at about -115 °C, followed by an exotherm recrystallization at about -63 °C peak temperature

Applicant's summary and conclusion