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Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2011-03-01 to 2011-05-10
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results.
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7200 (Melting Point / Melting Range)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Remarks:
Date of Inspection: 26 and 27 October 2010 Date of Signature: 8 February 2011
Type of method:
method to determine freezing temperature
Key result
Melting / freezing pt.:
< -50 °C
Remarks on result:
other: Atmospheric pressure was not reported.
Melting / freezing pt.:
< 223.15 K
Remarks on result:
other: Atmospheric pressure was not reported.

PERFORMANCE OF THE PRETEST

Calibration of the thermometer

The thermometer was checked against a certified thermometer. A correction did not need to be applied.

Preliminary test

The preliminary test was performed and no congestion was observed down to a temperature of - 50 °C.

Main Test

As no congealing was observed in the preliminary test, no further tests were undertaken

Conclusions:
No freezing point was observed down to a temperature of -50 °C (223.15 K). Therefore: Freezing point of Benzyl Salicylate was determined to be less than -50 °C (223.15 K).
Executive summary:
The freezing point of Benzyl Salicylate was measured according to the OECD guideline No. 102 (method of freezing temperature). No freezing was observed down to a temperature of -50 °C (223.15 K). Therefore, Freezing point of Benzyl Salicylate was determined to be less than -50 °C (223.15 K).

Description of key information

No freezing point was observed down to a temperature of -50 °C (223.15 K). Therefore: Freezing point of Benzyl Salicylate was determined to be less than -50 °C (223.15 K).

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-50 °C

Additional information