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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
15 February 2013 - 03 May 2013
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Cross-reference
Reason / purpose for cross-reference:
reference to same study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2013
Report date:
2013

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Version / remarks:
(2008)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Version / remarks:
(1995)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7220 (Boiling Point / Boiling Range)
Version / remarks:
(1996)
Deviations:
no
GLP compliance:
yes
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
Methyl 3-amino-5,6-dichloropyrazine-2-carboxylate
EC Number:
215-947-7
EC Name:
Methyl 3-amino-5,6-dichloropyrazine-2-carboxylate
Cas Number:
1458-18-0
Molecular formula:
C6H5Cl2N3O2
IUPAC Name:
methyl 3-amino-5,6-dichloropyrazine-2-carboxylate
Test material form:
solid: particulate/powder
Details on test material:
Identification: Amiloride Compound 7
Molecular formula: C6H5Cl2N3O2
Molecular weight: 222.03
CAS Number:1458-18-0
Description: Tan powder
Batch: 206-2
Purity/Composition: 99.7 area%
Test substance storage: In refrigerator (2-8°C) protected from light, desiccated
Stability under storage conditions: Stable
Expiry date: 11 May 2014 (Retest date)

Results and discussion

Boiling point
Remarks on result:
not determinable
Remarks:
Boiling of not observed below the temperature at which decomposition started.

Any other information on results incl. tables

Boiling of the test substance was not observed below the temperature at which decomposition started.

Applicant's summary and conclusion

Conclusions:
No boiling before decomposition was observed for Amiloride Compound 7 using differential scanning calorimetry (GLP-compliant study in accordance with EC A.2, OECD 103 and EPA OPPTS 830.7220). The substance has no boiling temperature.