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Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
comparable to guideline study
Justification for type of information:
Experimental test result performed using standard OECD test guidelines.
Qualifier:
according to guideline
Guideline:
other: as mentioned below
Principles of method if other than guideline:
The Freezing point of 1,4-dimethyl-5-[[4-[methylbenzylamino]phenyl]azo]-1H-1,2,4-triazolium acetate was determined.
GLP compliance:
not specified
Type of method:
other: crushed ice and salt method (Freezing Temperature Method)
Specific details on test material used for the study:
- Name of test material: 1,4-dimethyl-5-[[4-[methylbenzylamino]phenyl]azo]-1H-1,2,4-triazolium acetate
- IUPAC name: 1,4-dimethyl-5-[[4-[methylbenzylamino]phenyl]azo]-1H-1,2,4-triazolium acetate
- Molecular formula: C18H21N6.C2H3O2
- Molecular weight: 380.4496 g/mole
- Smiles : CC(=O)[O-].Cn1cn[n+](c1/N=N/c2ccc(cc2)N(C)Cc3ccccc3)C
- Inchl: 1S/C18H21N6.C2H4O2/c1-22(13-15-7-5-4-6-8-15)17-11-9-16(10-12-17)20-21-18-23(2)14-19-24(18)3;1-2(3)4/h4-12,14H,13H2,1-3H3;1H3,(H,3,4)/q+1;/p-1
- Substance type: Organic
- Physical state: Liquid
Key result
Melting / freezing pt.:
< -10.38 °C
Remarks on result:
other: no other details mentioned
Conclusions:
The Freezing point of 1,4-dimethyl-5-[[4-[methylbenzylamino]phenyl]azo]-1H-1,2,4-triazolium acetate was determined. No freezing was observed up to -10.38 °C. Hence, the freezing point was inferred to be less than -10.38°C.
Executive summary:

The Freezing point of 1,4-dimethyl-5-[[4-[methylbenzylamino]phenyl]azo]-1H-1,2,4-triazolium acetate was determined. No freezing was observed up to -10.38 °C. Hence, the freezing point was inferred to be less than -10.38°C.

Description of key information

The Freezing point of 1,4-dimethyl-5-[[4-[methylbenzylamino]phenyl]azo]-1H-1,2,4-triazolium acetate was determined. No freezing was observed up to -10.38 °C. Hence, the freezing point was inferred to be less than -10.38°C.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-10.38 °C

Additional information

The Freezing point of 1,4-dimethyl-5-[[4-[methylbenzylamino]phenyl]azo]-1H-1,2,4-triazolium acetate was determined. No freezing was observed up to -10.38 °C. Hence, the freezing point was inferred to be less than -10.38°C.