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Administrative data

Endpoint:
flash point of flammable liquids
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Experimental Starting Date: 28 May 2015 Experimental Completion Date: 08 June 2015
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2015
Report date:
2015

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.9 (Flash-Point)
Deviations:
no
GLP compliance:
yes
Type of method:
equilibrium method closed cup

Test material

Constituent 1
Chemical structure
Reference substance name:
(3S,6E)-3,7,11-trimethyldodeca-6,10-dienal
EC Number:
810-298-1
Cas Number:
194934-66-2
Molecular formula:
C15H26O
IUPAC Name:
(3S,6E)-3,7,11-trimethyldodeca-6,10-dienal
Test material form:
liquid

Results and discussion

Flash point
Key result
Flash point:
136 °C
Atm. press.:
99.7 kPa

Any other information on results incl. tables

Results

Results of the flash point determination are shown in the following table.

 

Table 3.1

 

Temperature (ºC)

Observations

20.0

No flash.

25.0

No flash.

30.0

No flash.

35.0

No flash.

40.0

No flash.

45.0

No flash.

50.0

No flash.

55.0

No flash.

60.0

No flash.

65.0

No flash.

70.0

No flash.

70.0 (fresh sample)

No flash.

75.0

No flash.

80.0

No flash.

85.0

No flash.

90.0

No flash.

95.0

No flash.

100.0

No flash.

105.0 (fresh sample)

No flash.

110.0

No flash.

115.0

No flash.

120.0

No flash. The test flame self-extinguished.

125.0

No flash.

130.0

No flash.

135.0

A blue flash spread across the sample cup.

135.0 (fresh sample)

No flash.

140.0

No flash.

 

Table 3.1 (continued)

 

Temperature (ºC)

Observations

145.0

No flash.

150.0

No flash.

155.0

No flash.

160.0

No flash. The test flame enlarged when dipped.

165.0

No flash. The test flame enlarged when dipped.

170.0

No flash. The test flame enlarged when dipped.

175.0

No flash. The test flame enlarged when dipped.

180.0

No flash. The test flame enlarged when dipped.

185.0

No flash. The test flame enlarged when dipped.

185.0 (fresh sample)

No flash. The test flame enlarged when dipped.

150.0 (fresh sample)

No flash. The test flame enlarged when dipped.

140.0 (fresh sample)

No flash. The test flame enlarged slightly when dipped.

136.0 (fresh sample)

No flash.

137.0 (fresh sample)

No flash. The test flame self-extinguished when dipped.

138.0 (fresh sample)

No flash. The test flame self-extinguished when dipped.

139.0 (fresh sample)

No flash.

140.0 (fresh sample)

A blue flash spread across the sample cup.

140.0 (fresh sample)

A blue flash spread across the sample cup.

138.0 (fresh sample)

A blue flash spread across the sample cup.

138.0 (fresh sample)

A blue flash spread across the sample cup.

136.0 (fresh sample)

A blue flash spread across the sample cup.

136.0 (fresh sample)

A blue flash spread across the sample cup.

134.0 (fresh sample)

No flash.

134.0 (fresh sample)

No flash.

 

Atmospheric pressure: 99.7 kPa

Corrected flash point: 136.37 ºC

 

Applicant's summary and conclusion

Interpretation of results:
GHS criteria not met
Conclusions:
The flash point of the test item has been determined to be 136 ± 2 °C.
Executive summary:

The determination was carried out using a closed cup flash point tester*, using a procedure designed to be compatible with Method A9 Flash Point of Commission Regulation (EC) No 440/2008 of 30 May 2008.

 

Instrument: Setaflash 30000-0 flash point tester


*Based on, Anon (1983) Paints, Varnishes, Petroleum and Related Products – Determination of Flash Point – Rapid Equilibrium Method,International Standard ISO 3679-2004 (E),Second Edition –2004-04-01,P1-18and Anon (1989) Flash Point of Liquids by Setaflash Closed-Cup Apparatus,ASTM D-3278-89,P1-7.

Conclusion

The flash point of the test item has been determined to be 136 ± 2 °C.

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