Registration Dossier
Registration Dossier
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EC number: 248-607-1 | CAS number: 27689-12-9
Melting point / freezing point
Administrative data
- Endpoint:
- melting point/freezing point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 07 Apr - 11 May 2015
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- other: Test procedure in accordance with national standard methods under GLP
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 015
- Report date:
- 2015
Materials and methods
Test guidelineopen allclose all
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 102 (Melting point / Melting Range)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.1 (Melting / Freezing Temperature)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- EPA OPPTS 830.7200 (Melting Point / Melting Range)
- Deviations:
- no
- GLP compliance:
- yes
- Type of method:
- thermal analysis
Test material
- Reference substance name:
- Procrylat
- IUPAC Name:
- Procrylat
- Details on test material:
- - Name of test material (as cited in study report): MTDID 9115
- Physical state: Clear colourless to yellowish liquid
- Analytical purity: 96%
- Expiration date of the lot/batch: 24 November 2015
- Storage condition of test material: at room temperature
Constituent 1
Results and discussion
Melting / freezing point
- Melting / freezing pt.:
- -41 °C
- Remarks on result:
- other: Pressure not reported
Any other information on results incl. tables
During cooling in Experiment 1, a glass transition was observed between -40 °C and -50 °C. During heating, a glass transition was observed between -50 °C and -25 °C. The inflection point of the glass transition was - 40.54 °C. Experiment 2 was performed as a duplicate of Experiment 1. Similar results as with Experiment 1 were obtained. The inflection point of the glass transition was -40.48 °C. The melting temperature (glass transition) was determined as the average melting temperature obtained from Experiment 1 (-40.54 °C) and Experiment 2 (-40.48 °C).
Applicant's summary and conclusion
- Conclusions:
- A melting point of -41 °C was observed for Procrylat as determined by the OECD 102 method.
- Executive summary:
The melting point of Procrylat was tested using differential scanning calorimetry (DSC). During cooling in both experiments, a glass transition was observed between -40 °C and -50 °C. During heating, a glass transition was observed between -50 °C and -25 °C. The average inflection point of the glass transition was -41 °C. The study was conducted in accordance with the OECD 102 method and was GLP compliant; therefore the study is considered reliable without restrictions.
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