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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
21 July 1992 - 4 February 1993
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Study conducted to GLP in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
1993
Report date:
1993

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
other: ASTM D1120-72
Deviations:
no
GLP compliance:
yes
Type of method:
ebulliometer

Test material

Constituent 1
Chemical structure
Reference substance name:
3,5-dimethylbenzoyl chloride
EC Number:
413-010-9
EC Name:
3,5-dimethylbenzoyl chloride
Cas Number:
6613-44-1
Molecular formula:
C9H9ClO
IUPAC Name:
3,5-dimethylbenzoyl chloride
Details on test material:
DMBC
Appearance: clear, colourless liquid
Storage conditions: room temperature in the dark

Results and discussion

Boiling point
Boiling pt.:
239 °C
Atm. press.:
1 009 mBar
Decomposition:
yes
Remarks:
The sample started to turn yellow at ca. 228 °C and became yellow/orange in colour during the course of the determination indicating partial decomposition.
Decomp. temp.:
ca. 228 °C
Remarks on result:
other: White smoke-like fumes were evolved which condensed to a clear colourless liquid in the condenser.

Any other information on results incl. tables

Test 1: 239.5 °C

Test 2: 238.5 °C

Applicant's summary and conclusion

Conclusions:
DMBC has a boiling point of 239 °C at atmospheric pressure.
Executive summary:

DMBC has a boiling point of 239 °C at atmospheric pressure. The test was conducted in accordance with EEC Method A2.