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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Study conducted in 2003 according to ASTM E537-86, Method A2 of the Commission Directive 92/69/EEC and in accordance with GLP. Study material is well characterized.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2005
Report date:
2005

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Version / remarks:
Commission Directive 92/69/EEC, A2 (differential scanning calorimetry method).
Deviations:
no
GLP compliance:
yes
Type of method:
differential scanning calorimetry

Test material

Test material form:
liquid

Results and discussion

Boiling point
Boiling pt.:
> 360 K
Atm. press.:
101.46 kPa
Decomposition:
yes
Remarks:
gradual decomposition
Decomp. temp.:
<= 517 K
Remarks on result:
other: value is a calculated boiling point

Any other information on results incl. tables

No discernable onset temperature was observed by DSC. Therefore onset temperarure was assessed by visual estimate.

Observation Temperature
 K
  sample was clear colorless liquid 296 
 sample was very pale straw colored liquid   517 
 sample was pale straw colored liquid    526
     sample appeared to be partially solidifying. Sample was pale straw colored liquid with solid particles present 527
    sample was light brown cloudy liquid with brown particles present  601
    sample was brown liquid with brown particles present     633

Applicant's summary and conclusion

Conclusions:
The test material has been determined to decompose gradually from 517 K at 101.46 kPa. As the test material decomposed, no value for the boiling point could be determined. A calculated value of boiling temperature gave a result of greater than 633 K.