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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes
Type of method:
differential scanning calorimetry
Remarks on result:
other: In the closed crucible, two endothermic phases were visible between approx. 43 °C – 75 °C and approx. 75 °C – 100 °C indicating a large melting range.
Conclusions:
Between 25 °C and 450 °C no definite melting could be observed by DTA/DSC method.
Executive summary:

Melting point to test item EGGE 2806-1 was analyzed DTA/DSC.

Between 25 °C and 450 °C no definite melting could be observed. Two endothermic effects were visible between approx. 45 °C – 80 °C and approx. 80 °C – 100 °C indicating a large melting range. From approx. 160 °C to 255 °C another endothermic effect was observed, which goes over in two exothermic effects from 255 °C up to 450 °C very probably indicating decomposition of the test item.

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes
Type of method:
capillary method
Key result
Melting / freezing pt.:
>= 90 - <= 100 °C
Remarks on result:
other: At approx. 100 °C sample transformed into a clear liquid, no solid particles were left

At about 40 °C the sample began to shrink partially. At about 90 °C the melting process of the shrunken sample started and was completed at approx. 100 °C ending with a clear liquid.

Conclusions:
Visual observation by capillary tube showed a melting range of approx. 90 - 100 °C to test item EGGE 2806-1.
Executive summary:

Melting point to test item EGGE 2806-1 was analyzed via capillary tube (visual oberservation).

At about 40 °C the sample began to shrink partially. At about 90 °C the melting process of the shrunken sample started and was completed at approx. 100 °C ending with a clear liquid.

Melting range: approx. 90 – 100 °C

Description of key information

Between 25 °C and 450 °C no definite melting could be observed by DTA/DSC method.

Visual observation by capillary tube showed a melting range of approx. 90 - 100 °C to test item EGGE 2806-1.

Key value for chemical safety assessment

Additional information