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Diss Factsheets

Physical & Chemical properties

Particle size distribution (Granulometry)

Administrative data

Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
1 July 1993 - 11 April 1994
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: GLP guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
1994
Report date:
1994

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
other: EC Directive 92/32/EEC
GLP compliance:
yes

Test material

Constituent 1
Chemical structure
Reference substance name:
Methyl O-(4-amino-3,5-dichloro-6-fluoropyridin-2-yloxy)acetate
EC Number:
407-550-4
EC Name:
Methyl O-(4-amino-3,5-dichloro-6-fluoropyridin-2-yloxy)acetate
Cas Number:
69184-17-4
Molecular formula:
Hill formula: C8 H7 Cl2 F N2 O3 CAS formula: C8 H7 Cl2 F N2 O3
IUPAC Name:
methyl 2-[(4-amino-3,5-dichloro-6-fluoropyridin-2-yl)oxy]acetate
Details on test material:
- Name of test material (as cited in study report): Fluroxypyr methyl ester
- Physical state: light grey moist powder
- Analytical purity: 93.6%
- Lot/batch No.: HJ11160402A
- Expiration date of the lot/batch: 18 November 1995
- Storage condition of test material: ambient temperature, in original container

Results and discussion

Particle size
Percentile:
D50
Remarks on result:
other: Migrated from fields under 'Mass median diameter' as D50 percentile. No source field for Standard deviation.
Particle size distribution at different passagesopen allclose all
No.:
#1
Size:
> 400 µm
Distribution:
64.1 %
No.:
#2
Size:
>= 125 - <= 400 µm
Distribution:
35.3 %
No.:
#3
Size:
>= 75 - <= 125 µm
Distribution:
0.3 %
No.:
#4
Size:
>= 30 - <= 75 µm
Distribution:
0.2 %
No.:
#5
Size:
>= 10 - <= 30 µm
Distribution:
0.1 %
No.:
#6
Size:
<= 10 µm
Distribution:
0.1 %

Any other information on results incl. tables

The results of the two series:

Particle size

(um)

% in range by weight

Test 1

Test 2

Mean

> 400

56.2

71.9

64.1

400-125

43.0

27.5

35.3

125-75

0.4

0.2

0.3

75-30

0.2

0.1

0.2

30-10

0.1

0.0

0.1

<10

0.1

0.0

0.1

Recovery

100.0

99.7

100.1

An insignificant amount of the test material is of particle size less than 10 um, with less than 1% of the test material of

particle size less than 125 um.

Applicant's summary and conclusion