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Diss Factsheets

Physical & Chemical properties

Particle size distribution (Granulometry)

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Reference
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
November 27, 2014
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
test procedure in accordance with generally accepted scientific standards and described in sufficient detail
Qualifier:
no guideline followed
Principles of method if other than guideline:
Laser Light Scattering. The particle size distribution was analysed using the Mastersizer 2000 tool, which used the technique of Laser Diffraction to measure the size of particles. It does this by measuring the intensity of Light Scattered as a Laser beam passes through a dispersed particulate sample. This data is then analysed to calculate the size of the particles that created the scattering pattern.
GLP compliance:
no
Type of method:
Laser scattering/diffraction
Type of distribution:
volumetric distribution
Key result
Percentile:
D50
Mean:
ca. 6.859 µm
Remarks on result:
other: St.deviation not reported
Percentile:
D10
Mean:
ca. 3.089 µm
Remarks on result:
other: St.deviation not reported
Percentile:
D90
Mean:
ca. 14.825 µm
Remarks on result:
other: St.deviation not reported

The analysis was done after two minutes of sample sonication.

Conclusions:
D10 = 3.089 µm
D50 = 6.859 µm
D90 = 14.825 µm
Executive summary:

Method


The particle size distribution was analysed using the Mastersizer 2000 tool, which used the technique of Laser Diffraction to measure the size of particles. It does this by measuring the intensity of Light Scattered as a Laser beam passes through a dispersed particulate sample. This data is then analysed to calculate the size of the particles that created the scattering pattern. The analysis was carried out after two minutes of sample sonication.


Results


D10 = 3.089 µm


D50 = 6.859 µm


D90 = 14.825 µm

Description of key information

Laser Light Scattering - Median Mass diameter = 6.859 µm

Additional information

D10 = 3.089 µm


D50 = 6.859 µm


D90 = 14.825 µm


 


Laser Light Scattering