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Diss Factsheets

Physical & Chemical properties

Particle size distribution (Granulometry)

Administrative data

Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Reported 03May2019
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
comparable to guideline study with acceptable restrictions

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2019
Report date:
2019

Materials and methods

Test guideline
Qualifier:
equivalent or similar to guideline
Guideline:
ISO 13320 (Particle size analysis - Laser diffraction methods)
GLP compliance:
no
Other quality assurance:
other: ISO9001
Type of method:
Laser scattering/diffraction
Type of particle tested:
primary particle
Type of distribution:
volumetric distribution

Test material

Constituent 1
Chemical structure
Reference substance name:
Methyl 1-methyl-4-[(methylphenylhydrazono)methyl]pyridinium sulphate
EC Number:
269-503-2
EC Name:
Methyl 1-methyl-4-[(methylphenylhydrazono)methyl]pyridinium sulphate
Cas Number:
68259-00-7
Molecular formula:
C14H16N3.CH3O4S
IUPAC Name:
methyl 1-methyl-4-[(methylphenylhydrazono)methyl]pyridinium sulphate
Test material form:
solid: particulate/powder
Details on test material:
See study reports for batch and purity information
Specific details on test material used for the study:
Basic Yellow 87
CI306087 1080982

Results and discussion

Particle sizeopen allclose all
Key result
Percentile:
D10
Mean:
ca. 31.9 µm
St. dev.:
0
Remarks on result:
other: St.Dev not reported
Key result
Percentile:
D50
Mean:
ca. 111 µm
St. dev.:
0
Remarks on result:
other: St.Dev not reported
Key result
Percentile:
D90
Mean:
ca. 364 µm
St. dev.:
0
Remarks on result:
other: St.Dev not reported

Applicant's summary and conclusion

Conclusions:
Particle size measurement was carried out on a Mastersizer 3000.
Specific Surface Area 41.36m2/kg
Particle Size
DV10 = 31.9 μm
DV50 = 111 μm
DV90 = 364 μm

According to measurement results obtained by the method and the definition, the reference mentioned is not considered above as a nanomaterial.
Executive summary:

Particle size measurement was carried out on a Mastersizer 3000.

The measured Specific Surface Area was 41.36m2/kg.

Particle Size distribution by volume was also measure with the results presented below.

DV10 = 31.9 μm

DV50 = 111 μm

DV90 = 364 μm

According to measurement results obtained by the method and the definition, the reference mentioned is not considered above as a nanomaterial.