Registration Dossier

Data platform availability banner - registered substances factsheets

Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2012-10-26 to 2013-06-17
Reliability:
1 (reliable without restriction)

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2013
Report date:
2013

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Version / remarks:
, 27 July 1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
other: The Guidelines for testing of chemicals" State Environmental Protection Administration (SEPA) of China, No.103
Deviations:
no
Principles of method if other than guideline:
Atmospheric pressure 89.98 kPa
GLP compliance:
no
Type of method:
method according to Siwoloboff

Test material

Constituent 1
Reference substance name:
Isopropylmagnesium chloride
IUPAC Name:
Isopropylmagnesium chloride
Constituent 2
Chemical structure
Reference substance name:
Chloro(1-methylethyl)magnesium
EC Number:
213-947-1
EC Name:
Chloro(1-methylethyl)magnesium
Cas Number:
1068-55-9
Molecular formula:
C3H7ClMg
IUPAC Name:
chloro(1-methylethyl)magnesium
Test material form:
other: liquid: Isopropylmagnesium chloride ca. 20% in Tetrahydrofuran

Results and discussion

Boiling point
Boiling pt.:
ca. 62.4 °C
Atm. press.:
ca. 89.98 kPa

Applicant's summary and conclusion

Conclusions:
The boiling point of Isopropylmagnesium chloride ca. 20% in THF was 62.4°C under 89.98kPa atmospheric pressure.
As the atmospheric pressure of the measured boiling point was not in the range of +/- 5 kPa to the standard atmospheric pressure (101.325 kPa) the calculation to normal boiling point according to the equation of Sidney Young is not feasible.