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Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2011-10-24 till 2011-10-31
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Version / remarks:
adopted 27 July 1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Version / remarks:
dated 31 May 2008
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7220 (Boiling Point / Boiling Range)
Version / remarks:
dated August 1996
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
method according to Siwoloboff
Key result
Boiling pt.:
> 400 °C
Atm. press.:
1 013.25 hPa
Remarks on result:
other: No boiling point according to the criteria described in the guideline could be observed up to 400 °C.
Conclusions:
No boiling point according to the criteria described in the guideline could be observed up to 400 °C for potassium hexadecyl hydrogen phosphate.
Executive summary:

A study was conducted according to Regulation (EC) No 440/2008 method A.2, OECD TG 103 and OPPTS 830.7220 08.1996. The determination of the boiling point was performed by visual judgement using the capillary method according to Siwoloboff. In two preliminary tests up to 400 °C a change of appearance and consistency of the test item was observed, but a boiling point according to the criteria described in the guideline was not observed. An additional main test was performed in the temperature range from 230 °C up to 400 °C with a heating rate of 1 °C. At start temperature the test item was liquid. During the test the colour of the test item changed from colourless to milky white. No clear boiling point as described in the guideline could be observed.

Description of key information

Up to 400 °C no clear boiling point could be observed for potassium hexadecyl hydrogen phosphate.

Key value for chemical safety assessment

Additional information

A study was conducted according to Regulation (EC) No 440/2008 method A.2, OECD TG 103 and OPPTS 830.7220 08.1996. The determination of the boiling point was performed by visual judgement using the capillary method according to Siwoloboff. In two preliminary tests up to 400 °C a change of appearance and consistency of the test item was observed, but a boiling point according to the criteria described in the guideline was not observed. An additional main test was performed in the temperature range from 230 °C up to 400 °C with a heating rate of 1 °C. At start temperature the test item was liquid. During the test the colour of the test item changed from colourless to milky white. No clear boiling point as described in the guideline could be observed.