Registration Dossier

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018

Materials and methods

Test guideline
Qualifier:
according to
Guideline:
OECD Guideline 103 (Boiling Point)
GLP compliance:
yes
Type of method:
ebulliometer

Test material

Reference
Name:
Unnamed
Type:
Constituent
Test material form:
liquid
Specific details on test material used for the study:
Test Item Name Tyzor TE
IUPAC Name titanium 2,2',2''-nitrilotrisethanolate
CAS No. 15879-01-3
EC No. 240-015-1
Batch number 334-300161/000004
Appearance Light yellow liquid
Manufactured by Dorf Ketal Speciality Catalyst Pvt Limited
Supplied to JRF by Dorf Ketal Speciality Catalyst Pvt Limited
Date of manufacture August 2017
Date of Expiry August 2019

Results and discussion

Boiling point
Key result
Boiling pt.:
> 89.7 - < 91.8 °C
Atm. press.:
ca. 760 mm Hg
Decomposition:
no

Any other information on results incl. tables

Boiling Point/Boiling Range of TYZOR TE

 

TABLE1:Boiling Point/Boiling RangeValues ofTYZOR TE

 

Atmospheric Pressure (760 mmHg)

Repli-cation

Temperature

of Initiation of Bubble Formation (°C)

Temperature at which Continuous String of Bubbles were Observed (°C)

Boiling Range

 (°C)

Boiling Point

(°C)

Kelvin (K)

R1

89.70

91.60

89.70 – 91.80

91.60

364.75

R2

89.80

91.80

91.80

364.95

R3

89.70

91.50

91.50

364.65

Mean

91.63

364.78

Standard Deviation

0.15

0.15


Typical Calculation

Boiling Point [in Kelvin (K)]    = Observed Boiling Point(°C) + 273.15

                                                         = 91.60 + 273.15

                                                         = 364.75


 

Applicant's summary and conclusion

Executive summary:

EXECUTIVE SUMMARY:

The boiling point of TYZOR TE was determined by following Siwoloboff method.

The boiling point of TYZOR TE was 364.75, 364.95 and 364.65 K at normal atmospheric pressure (760 mm Hg).

The mean boiling point of TYZOR TE was 364.78 ± 0.15 K (91.63 ± 0.15 °C) at normal atmospheric pressure (760 mm Hg) [TABLE 1].

The mean boiling range of TYZOR TE was 89.70 – 91.80 °C at normal atmospheric pressure (760 mm Hg).