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Physical & Chemical properties

Particle size distribution (Granulometry)

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Reference
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2018-01-18 to 2018-05-18
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 110 (Particle Size Distribution / Fibre Length and Diameter Distributions - Method A: Particle Size Distribution (effective hydrodynamic radius)
Qualifier:
according to guideline
Guideline:
ISO 13320 (Particle size analysis - Laser diffraction methods)
Qualifier:
according to guideline
Guideline:
other: CIPAC MT 187: Particle Size Analysis by Laser Diffraction
GLP compliance:
no
Type of method:
Laser scattering/diffraction
Type of particle tested:
agglomerate
Type of distribution:
volumetric distribution
Percentile:
D50
Mean:
1.951 µm
St. dev.:
0.16
Percentile:
D10
Mean:
0.552 µm
St. dev.:
0
Percentile:
D90
Mean:
184.3 µm
St. dev.:
77.8

The test item consisted of non-transparent particles that tended to agglomeration. The agglomeration influenced the test results.

Median particle size D (v, 0.5): 50% of particle volume or particle mass with lower particle diameter

1st test series: 1.926 µm

2nd test series: 1.975 µm

Average of the median particle size: 1.951 µm (standard deviation: 0.16 µm)

Particle size D (v, 0.1): 10% of particle volume or particle mass with lower particle diameter

1st test series: 0.553 µm

2nd test series: 0.550 µm

Average of the particle size: 0.552 µm (standard deviation: 0.00 µm)

Particle size D (v, 0.9): 90% of particle volume or particle mass with lower particle diameter

1st test series: 162.9 µm

2nd test series: 205.7 µm

Average of the particle size: 184.3 µm (standard deviation: 77.8 µm)

The particle size distribution showed a polymodal distribution with two maxima and two shoulders. The first maximum was observed at approximately 1.5 µm and the second at approximately 200 µm. The shoulders were observed at approximately 0.3 µm and at approximately 10 µm. The second measurement additionally showed a third shoulder at approximately 350 µm.

Conclusions:
The particle size distribution of the test item was determined by laser diffraction (light scattering):
Average of the median particle size D (v, 0.5): 1.951 µm (standard deviation: 0.16 µm)
Average of the particle size D (v, 0.1): 0.552 µm (standard deviation: 0.00 µm)
Average of the particle size D (v, 0.9): 184.3 µm (standard deviation: 77.8 µm)
Executive summary:

The particle size distribution of the test item was determined by laser diffraction (light scattering). The test item consisted of non-transparent particles that tended to agglomeration. The agglomeration influenced the test results.

Average of the median particle size D (v, 0.5): 1.951 µm (standard deviation: 0.16 µm)

Average of the particle size D (v, 0.1): 0.552 µm (standard deviation: 0.00 µm)

Average of the particle size D (v, 0.9): 184.3 µm (standard deviation: 77.8 µm)

Description of key information

The particle size distribution of the test item was determined by laser diffraction (light scattering).The test item consisted of non-transparent particles that tended to agglomeration. The agglomeration influenced the test results.

Average of the median particle size D (v, 0.5): 1.951 µm (standard deviation: 0.16 µm)

Average of the particle size D (v, 0.1): 0.552 µm (standard deviation: 0.00 µm)

Average of the particle size D (v, 0.9): 184.3 µm (standard deviation: 77.8 µm)

Additional information