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Physical & Chemical properties

Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
20 June 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
2008
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
capillary method
Key result
Melting / freezing pt.:
> 400 °C
Decomposition:
no
Remarks on result:
other: No melting point was observed up to 400 °C.

- No melting point was observed up to 400 °C.

- No physical change of colour or form was observed, there was no visual indication of decomposition.

Conclusions:
Under the conditions of this study, no melting point for the test material was observed up to 400 °C. No physical change of colour or form was observed, there was no visual indication of decomposition.
Executive summary:

The melting point of the test material was investigated in accordance with the standardised guidelines OECD 102 and EU Method A.1, under GLP conditions using the capillary method.

For the main study three capillaries containing the test material were placed into the apparatus, the block was heated from 390 to 400 °C at 0.5 °C/min heating rate. The transformations of the test material were observed, visually through the magnifying glass. Three parallel experiments were carried out and in each case three parallel samples were measured.

Under the conditions of this study, no melting point for the test material was observed up to 400 °C. No physical change of colour or form was observed, there was no visual indication of decomposition.

Description of key information

Under the conditions of this study, no melting point for the test material was observed up to 400 °C. No physical change of colour or form was observed, there was no visual indication of decomposition.

Key value for chemical safety assessment

Additional information

The melting point of the test material was investigated in accordance with the standardised guidelines OECD 102 and EU Method A.1, under GLP conditions using the capillary method. The study was awarded a reliability score of 1 in accordance with the criteria set forth by Klimisch et al. (1997).

For the main study three capillaries containing the test material were placed into the apparatus, the block was heated from 390 to 400 °C at 0.5 °C/min heating rate. The transformations of the test material were observed, visually through the magnifying glass. Three parallel experiments were carried out and in each case three parallel samples were measured.

Under the conditions of this study, no melting point for the test material was observed up to 400 °C. No physical change of colour or form was observed, there was no visual indication of decomposition.