Registration Dossier
Registration Dossier
Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.
The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.
Use of this information is subject to copyright laws and may require the permission of the owner of the information, as described in the ECHA Legal Notice.
EC number: 251-528-5 | CAS number: 33454-82-9
Melting point / freezing point
Administrative data
- Endpoint:
- melting point/freezing point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- March 2014
- Reliability:
- 2 (reliable with restrictions)
- Rationale for reliability incl. deficiencies:
- test procedure in accordance with national standard methods with acceptable restrictions
- Remarks:
- Protocol similar to OECD Guideline 103 and EU Method A.2 but limited documentation.
Cross-reference
- Reason / purpose for cross-reference:
- reference to same study
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 016
- Report date:
- 2016
Materials and methods
- Principles of method if other than guideline:
- DSC analysis
- GLP compliance:
- no
- Type of method:
- differential scanning calorimetry
Test material
- Reference substance name:
- Lithium trifluoromethanesulphonate
- EC Number:
- 251-528-5
- EC Name:
- Lithium trifluoromethanesulphonate
- Cas Number:
- 33454-82-9
- Molecular formula:
- CHF3O3S.Li
- IUPAC Name:
- lithium trifluoromethanesulphonate
- Test material form:
- solid: particulate/powder
- Details on test material:
- See confidential details on test material
Constituent 1
Results and discussion
Melting / freezing point
- Key result
- Melting / freezing pt.:
- > 422 °C
- Decomposition:
- yes
- Decomp. temp.:
- 422 °C
- Remarks on result:
- other:
- Remarks:
- The substance decomposes ate around 422°C before melting
Any other information on results incl. tables
A very small peak was observed from 134.8°C with a maximum at 138.6°C, associated to a very small endothermic decomposition of 19.85 J/g.
A second peak was observed from 410.3°C with a maximum at 422°C, associated to an endothermic decomposition of 110.2 J/g.
These peaks were not observed in the second heating run so they are associated to decomposition.
The DSC curve is available in the attached document.
Applicant's summary and conclusion
- Conclusions:
- Lithium Trifluoromethanesulfonate decomposes at 422°C before melting.
- Executive summary:
The determination of the melting point of the test substance was performed by a differential scanning calorimetry but with a limited documentation.
The test item was placed in crucible and was heated up to 450°C (heating rate: 10°C/min).
According to the DSC results, Lithium Trifluoromethanesulfonate decomposes before melting at 422°C.
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
Reproduction or further distribution of this information may be subject to copyright protection. Use of the information without obtaining the permission from the owner(s) of the respective information might violate the rights of the owner.
