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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
08 September 2010
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
study well documented, meets generally accepted scientific principles, acceptable for assessment
Qualifier:
equivalent or similar to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Principles of method if other than guideline:
The sample is filled into a test tube and is heated in the light path via a IR light barrier. The transmission is detected. As soon as the sample is clearly melted, the transmission jumps up and is showing the end of the melting process (here: transmission >= 40 %).
GLP compliance:
no
Other quality assurance:
other: ISO 9001:2008; FAMI-QS
Type of method:
other: capillary tube with photocell detection
Specific details on test material used for the study:
Batch No. 11510, 11511, 11512
Melting / freezing pt.:
>= 111.1 - <= 111.3 °C
Atm. press.:
101.3 kPa
Decomposition:
no

Test results

 Test Description  Result for Batch      
   11510  11511  11512

 Melting range starting point

 111.1

 111.2

 111.1

 Melting range ending point

 111.2

 111.3

 111.2

Description of key information

The substance dehydroacetic acid has a melting point of 111.1 -111.3 °C (capillary method).

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
111.1 °C

Additional information