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EC number: 812-877-4 | CAS number: 1228350-17-1
- Life Cycle description
- Uses advised against
- Endpoint summary
- Appearance / physical state / colour
- Melting point / freezing point
- Boiling point
- Density
- Particle size distribution (Granulometry)
- Vapour pressure
- Partition coefficient
- Water solubility
- Solubility in organic solvents / fat solubility
- Surface tension
- Flash point
- Auto flammability
- Flammability
- Explosiveness
- Oxidising properties
- Oxidation reduction potential
- Stability in organic solvents and identity of relevant degradation products
- Storage stability and reactivity towards container material
- Stability: thermal, sunlight, metals
- pH
- Dissociation constant
- Viscosity
- Additional physico-chemical information
- Additional physico-chemical properties of nanomaterials
- Nanomaterial agglomeration / aggregation
- Nanomaterial crystalline phase
- Nanomaterial crystallite and grain size
- Nanomaterial aspect ratio / shape
- Nanomaterial specific surface area
- Nanomaterial Zeta potential
- Nanomaterial surface chemistry
- Nanomaterial dustiness
- Nanomaterial porosity
- Nanomaterial pour density
- Nanomaterial photocatalytic activity
- Nanomaterial radical formation potential
- Nanomaterial catalytic activity
- Endpoint summary
- Stability
- Biodegradation
- Bioaccumulation
- Transport and distribution
- Environmental data
- Additional information on environmental fate and behaviour
- Ecotoxicological Summary
- Aquatic toxicity
- Endpoint summary
- Short-term toxicity to fish
- Long-term toxicity to fish
- Short-term toxicity to aquatic invertebrates
- Long-term toxicity to aquatic invertebrates
- Toxicity to aquatic algae and cyanobacteria
- Toxicity to aquatic plants other than algae
- Toxicity to microorganisms
- Endocrine disrupter testing in aquatic vertebrates – in vivo
- Toxicity to other aquatic organisms
- Sediment toxicity
- Terrestrial toxicity
- Biological effects monitoring
- Biotransformation and kinetics
- Additional ecotoxological information
- Toxicological Summary
- Toxicokinetics, metabolism and distribution
- Acute Toxicity
- Irritation / corrosion
- Sensitisation
- Repeated dose toxicity
- Genetic toxicity
- Carcinogenicity
- Toxicity to reproduction
- Specific investigations
- Exposure related observations in humans
- Toxic effects on livestock and pets
- Additional toxicological data
Boiling point
Administrative data
- Endpoint:
- boiling point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- August 24-September 27, 2016
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 016
- Report date:
- 2016
Materials and methods
Test guideline
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 103 (Boiling Point)
- Version / remarks:
- adopted July 27, 1995
- Deviations:
- no
- GLP compliance:
- yes (incl. QA statement)
- Type of method:
- method according to Siwoloboff
Test material
- Reference substance name:
- 4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononyl methacrylate
- EC Number:
- 812-877-4
- Cas Number:
- 1228350-17-1
- Molecular formula:
- C13 H11 F13 O2
- IUPAC Name:
- 4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononyl methacrylate
- Test material form:
- liquid
- Details on test material:
- Test Item name Fluowet PMA600
Batch No. DH213/16
Appearance transparent to brownish liquid
Purity 99.4 %
Expiry date 01 June 2017
Storage room temperature, protected from light
Constituent 1
- Specific details on test material used for the study:
- Test Item name Fluowet PMA600
Batch No. DH213/16
Appearance transparent to brownish liquid
Purity 99.4 %
Expiry date 01 June 2017
Storage room temperature, protected from light
Results and discussion
Boiling pointopen allclose all
- Key result
- Boiling pt.:
- 232.9 °C
- Atm. press.:
- > 100.45 - < 100.51 kPa
- Decomposition:
- no
- Remarks on result:
- other: at ambient atmosperic pressure
- Key result
- Boiling pt.:
- 506 K
- Atm. press.:
- > 100.45 - < 100.51 kPa
- Decomposition:
- no
- Remarks on result:
- other: at ambient atmospheric pressure
Any other information on results incl. tables
Reference test
The checking of apparatus with Ultrapure Water
29 August 2016 |
|
Atmospheric pressure, kPa |
Boiling point, °C |
99.78 |
100.1 |
98.78 |
99.9 |
99.78 |
100.0 |
Mean: |
100.0 |
|
|
31 August 2016 |
|
Atmospheric pressure, kPa |
Boiling point, °C |
100.51 |
100.2 |
100.51 |
100.1 |
100.50 |
100.1 |
Mean: |
100.1 |
The boiling point of Ultrapure Water was determined to be 100.0 and 100.1 °C. Measured values were determined to be in the required range (literature value ± 0.5°C).
Preliminary test was performed before the main test. Glass tube filled with test item was heated from 30 °C up to the boiling point at a rate of 5 °C/min.
Preliminary test
Start temperature, |
Heating rate |
Atmospheric pressure, kPa |
Boiling point, °C |
30 |
5 |
99.77 |
222.5 |
Determination of the Boiling Point of Fluowet PMA600
Atmospheric pressure, kPa |
Boiling point, °C |
Boiling point, K |
100.48 |
233.1 |
506.25 |
100.51 |
233.3 |
506.45 |
100.45 |
232.2 |
505.35 |
Mean: |
232.9 |
506.0 |
RSD (CV%): |
0.3 |
- |
Conf.int. (95%): |
1.46 |
- |
Applicant's summary and conclusion
- Conclusions:
- The boiling point of Fluowet PMA600 was determined to be 506.0 K (232.9 °C).
- Executive summary:
The boiling point is determined using a method following Siwoloboff with automatic photo-electrical detection. The test item was filled into a sample tube containing a capillary tube in such a manner that the sealed part of the capillary was lying below the surface of the test item. The tube was inserted in the center opening of the melting point apparatus. The atmospheric pressure was recorded before the measurement. Based on the preliminary test the metal block was heated up to 12 °C below the expected boiling point. The block was heated from 210 °C at 0.5 °C/min heating rate.When bubbles rose constantlyon the boiling capillary,the boiling point was determined with automatic photo-electrical detection. The experiment was performed in triplicate. The mean of the replicates was calculated and reported.
The boiling point of Fluowet PMA600 was determined to be 232.9 °C i.e. 506.0 K.
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