2,4-Thiophenedicarbonitrile, 5-amino-3-methyl-

Melting point / freezing point

Administrative data

Endpoint:

melting point/freezing point

Type of information:

experimental study

Adequacy of study:

key study

Study period:

5 April 2010

Reliability:

2 (reliable with restrictions)

Rationale for reliability incl. deficiencies:

other: Study conducted in accordance with generally accepted scientific principles, possibly with incomplete reporting or methodological deficiencies, which do not affect the quality of the relevant results.

Data source

Reference

Reference Type:

study report

Title:

Unnamed

Year:

2010

Report date:

2010

Materials and methods

Test guideline

Qualifier:

according to guideline

Guideline:

OECD Guideline 102 (Melting point / Melting Range)

Deviations:

no

GLP compliance:

no

Type of method:

capillary method

Test material

Test material information

Constituent 1

Reference substance name:

5-amino-3-methylthiophene-2,4-dicarbonitrile

EC Number:

610-868-8

Cas Number:

52603-48-2

Molecular formula:

C7N3H5S

IUPAC Name:

5-amino-3-methylthiophene-2,4-dicarbonitrile

Results and discussion

Melting / freezing point

Melting / freezing pt.:

225.13 °C

Decomposition:

no

Sublimation:

no

Any other information on results incl. tables

No atmospheric pressure for the test was provided.

Table 1: Temperatures at which each of the above stages occured.

	STAGE
Measurement	A	B	C	D	E
1	224.00^oC	224.25^oC	224.50^oC	224.80^oC	225.00^oC
2	223.50^oC	224.00^oC	224.25^oC	225.00^oC	225.25^oC

Applicant's summary and conclusion

Conclusions:

The test compound was found to have an average melting point of 225.13 °C.

Executive summary:

In a melting point determination study (KP04052010), the average melting point of the test material was determined to be 225.13 °C, according to OECD test Method 102.