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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
guideline study with acceptable restrictions
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Type of method:
capillary method
Melting / freezing pt.:
>= 52.8 - <= 57 °C
Remarks on result:
other: atmospheric pressure is reported
Conclusions:
A melting range of 53 - 57 °C is determined for the test substance at atmospheric pressure.
Executive summary:

A study was conducted to determine the melting point of the test substance according to EU method A.1. A small amount of the finely ground substance (dried for 24 h in an exsiccator) is placed in a capillary tube and packed tightly. The tube is heated, together with a thermometer in an oil bath, and the temperature rise is adjusted to less than about 1 K/min during the actual melting (starting temperature 33 °C).

A melting range of 52.8 - 57 °C is determined for the test substance at atmospheric pressure.

Description of key information

A study was conducted to determine the melting point of the test substance according to EU method A.1. A small amount of the finely ground substance (dried for 24 h in an exsiccator) is placed in a capillary tube and packed tightly. The tube is heated, together with a thermometer in an oil bath, and the temperature rise is adjusted to less than about 1 K/min during the actual melting (starting temperature 33 °C).

A melting range of 52.8 - 57.0 °C is determined for the test substance at atmospheric pressure.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
52.8 °C

Additional information