Registration Dossier
Registration Dossier
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EC number: 308-020-4 | CAS number: 97808-97-4
Melting point / freezing point
Administrative data
- Endpoint:
- melting point/freezing point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 8th August 2019 - 11th September 2019
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 019
- Report date:
- 2019
Materials and methods
Test guidelineopen allclose all
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 102 (Melting point / Melting Range)
- Version / remarks:
- Adopted 27 July 1995
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.1 (Melting / Freezing Temperature)
- Version / remarks:
- 31 May 2008
- Deviations:
- no
- GLP compliance:
- yes (incl. QA statement)
- Type of method:
- capillary method
Test material
- Reference substance name:
- Water
- EC Number:
- 231-791-2
- EC Name:
- Water
- Cas Number:
- 7732-18-5
- Molecular formula:
- H2O
- IUPAC Name:
- Water
- Reference substance name:
- C12-C14 alcohol
- IUPAC Name:
- C12-C14 alcohol
- Reference substance name:
- Mono (C12-C14 alkyl) phosphate ester
- IUPAC Name:
- Mono (C12-C14 alkyl) phosphate ester
- Reference substance name:
- Di (C12-C14 alkyl) diphosphate ester
- IUPAC Name:
- Di (C12-C14 alkyl) diphosphate ester
- Reference substance name:
- Tri (C12-C14 alkyl) triphosphate ester
- IUPAC Name:
- Tri (C12-C14 alkyl) triphosphate ester
- Reference substance name:
- C12-C14 alkyl pyrophosphate esters
- IUPAC Name:
- C12-C14 alkyl pyrophosphate esters
- Reference substance name:
- Ortho-phosphoric acid
- IUPAC Name:
- Ortho-phosphoric acid
- Reference substance name:
- unknown
- Molecular formula:
- unknown
- IUPAC Name:
- unknown
- Test material form:
- solid: bulk
Constituent 1
Constituent 2
Constituent 3
Constituent 4
Constituent 5
Constituent 6
Constituent 7
Constituent 8
- Specific details on test material used for the study:
- CAS Number: 68412-59-9
Physical Appearance: Solid whitish
Batch No. l023S l 7201
Purity% (As per CoA): 98.7%
Date of Manufacture: 21/06/2016
Date of Expiry: 09/07/2020
Storage Condition: Ambient (21 to 29°C)
Results and discussion
Melting / freezing pointopen allclose all
- Melting / freezing pt.:
- ca. 33.2 °C
- Remarks on result:
- other: Replica 1
- Melting / freezing pt.:
- ca. 33.5 °C
- Remarks on result:
- other: Replica 2
- Melting / freezing pt.:
- ca. 33.4 °C
- Remarks on result:
- other: Replica 3
- Key result
- Melting / freezing pt.:
- ca. 33.37 °C
- Remarks on result:
- other: Mean of triplicate 33.37 with 0.46% RSD.
Any other information on results incl. tables
The melting point for the preliminary experiment was 34.5°C.
Applicant's summary and conclusion
- Conclusions:
- The melting point of the substance was found to be 33.37°C with 0.46% of RSD.
- Executive summary:
The study was performed in accordance with OECD guideline No. 102, "Melting Point/Melting Range" using digital melting point apparatus. Melting point of triplicate samples has been determined as 33.37 ± 0.10 °C with 0.46% of RSD.
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