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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
supporting study
Reliability:
4 (not assignable)
Rationale for reliability incl. deficiencies:
other: Information from an example of patent literature based on fraction distillation process; no further information is available. Not under GLP, basic data given.

Data source

Reference
Reference Type:
other: experimental result of fractional distillation
Title:
Unnamed
Year:
1972
Report date:
1972

Materials and methods

Principles of method if other than guideline:
fractional distillation
GLP compliance:
no
Type of method:
distillation method

Test material

Constituent 1
Reference substance name:
methyl 2-phenyl-2-(dimethylamino)-butyrate
IUPAC Name:
methyl 2-phenyl-2-(dimethylamino)-butyrate
Test material form:
other: liquid
Details on test material:
distillate of an extract manufactured accordimg to example 3 of the patent

Results and discussion

Boiling point
Boiling pt.:
>= 90 - <= 95 °C
Atm. press.:
ca. 1 mm Hg

Any other information on results incl. tables

no data

Applicant's summary and conclusion

Conclusions:
The boiling point is 90-95 °C at 1 mm.
Executive summary:

The boiling point of 90-95 °C at 1 mm is reported in a patent example as a result of a fractional distillation only.

Hence, the information on boiling point of methyl 2-(dimethylamino)-2-phenylbutyrate is considered to be not assignable.