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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
02 March 2018
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
guideline study with acceptable restrictions
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
1995
Deviations:
no
GLP compliance:
no
Type of method:
differential scanning calorimetry
Key result
Melting / freezing pt.:
341 °C
Decomposition:
yes
Decomp. temp.:
445 °C
Remarks on result:
other: no information on atm pressure provided

- The onset of melting was at 339.4 °C, the peak was at 341.1 °C with + 14.9 J/g² energy (endotherm.).

- The test material melted at 341 °C .

Conclusions:
Under the conditions of this study, the test material melted at 341 °C .
Executive summary:

The melting point of the test material was determined in accordance with the standardised guideline OECD 102, using differential scanning calorimetry.

The prepared crucibles (crucible with test material and reference crucible) were placed in the DSC apparatus. Both crucibles were heated up from room temperature to 500 °C with a heating rate of 5 K/min.

The onset of melting was at 339.4 °C, the peak was at 341.1 °C with + 14.9 J/g² energy (endotherm.).

Under the conditions of this study, the test material melted at 341 °C .

Description of key information

Under the conditions of this study, the test material melted at 341 °C .

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
341 °C

Additional information

The melting point of the test material was determined in accordance with the standardised guideline OECD 102, using differential scanning calorimetry. The study was awarded a reliability score of 2 in accordance with the criteria set forth by Klimisch et al. (1997).

The prepared crucibles (crucible with test material and reference crucible) were placed in the DSC apparatus. Both crucibles were heated up from room temperature to 500 °C with a heating rate of 5 K/min.

The onset of melting was at 339.4 °C, the peak was at 341.1 °C with + 14.9 J/g² energy (endotherm.).

Under the conditions of this study, the test material melted at 341 °C .