Registration Dossier

Data platform availability banner - registered substances factsheets

Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2008
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2008
Report date:
2008

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
1992
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
1995
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
other: DSC

Test material

Constituent 1
Chemical structure
Reference substance name:
methyl cis-1-{[(2,5-dimethylphenyl)acetyl]amino}-4-methoxycyclohexanecarboxylate
EC Number:
606-524-1
Cas Number:
203313-47-7
Molecular formula:
C19H27NO4
IUPAC Name:
methyl cis-1-{[(2,5-dimethylphenyl)acetyl]amino}-4-methoxycyclohexanecarboxylate
Test material form:
solid: bulk

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
99.8 °C
Decomposition:
no
Remarks on result:
other: No atmospheric pressure is stated.

Any other information on results incl. tables

Two DSC-runs in aluminium crucibles with a hole showed an endothermic effect (melting) in the temperature range 90 - 115 °C with an onset temperature of 100 °C. The onset temperature is derived from the intersection of the tangent line with the highest slope of the endothermic peak with the baseline.

Applicant's summary and conclusion

Conclusions:
The test item had a melting point of 99.8 °C.
Executive summary:

The test item had a melting point of 99.8 °C.