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Diss Factsheets

Physical & Chemical properties

Particle size distribution (Granulometry)

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Reference
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
02. - 04. May 2018
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
study well documented, meets generally accepted scientific principles, acceptable for assessment
Qualifier:
no guideline followed
Principles of method if other than guideline:
The Mastersizer 3000 uses the technique of laser diffraction to measure the size of particles. It does this by measuring the intensity of light scattered as a laser beam passes through a dispersed particulate sample. This data is then analyzed to calculate the size of the particles that created the scattering pattern.
GLP compliance:
no
Type of method:
Laser scattering/diffraction
Type of particle tested:
primary particle
Type of distribution:
volumetric distribution
Specific details on test material used for the study:
samples from 12 different transport batches are used for the study:
Key result
Percentile:
D50
Mean:
8.44 µm
St. dev.:
1.23
Key result
Percentile:
D10
Mean:
2.29 µm
St. dev.:
0.39
Key result
Percentile:
D90
Mean:
18.59 µm
St. dev.:
2.5
Conclusions:
A mean Dv (50) of 8.44 µm is obtained.

Description of key information

Information on particle size of the substance is available from analytical determination of 12 different transport batches.

the volumetric distribution was determined, The mean Dv (50) is 8.44 µm.

Additional information