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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Testing was conducted between 19 February 2010 and 14 April 2010.
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2010
Report date:
2010

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Reference substance name:
Paraffin waxes and Hydrocarbon waxes, chloro, sulfochlorinated
EC Number:
269-145-7
EC Name:
Paraffin waxes and Hydrocarbon waxes, chloro, sulfochlorinated
Cas Number:
68188-19-2
Molecular formula:
CnHxCly(SO2Cl)z n= 14 - 17 or n=17 - 30 ; x=2n+2-y-z
IUPAC Name:
Paraffin waxes and Hydrocarbon waxes, chloro, sulfochlorinated
Constituent 2
Reference substance name:
SULFOCLOR LF 1013
IUPAC Name:
SULFOCLOR LF 1013
Details on test material:
Sponsor's identification: SULFOCLOR LF 1013
CAS No : 68188-19-2
Description : pale yellow slightly viscous liquid
Purity : >99%
Batch number : not supplied
Label : Sulfoclor LF 1013 TANQUE 25.09.2009
Date received : 05 February 2010
Expiry date : 23 September 2010
Storage conditions: room temperature in the dark

Results and discussion

Boiling point
Atm. press.:
99.21 kPa
Decomposition:
yes
Decomp. temp.:
438 K
Remarks on result:
other: As Sulfoclor LF 1013 decomposed, no value for boiling temperature could be determined experimentally.

Any other information on results incl. tables

Thermographic data for determinations 1 and 2 are in the following tables.

Thermographic Data – Determination 1

Thermal Event

Interpretation

Temperature

ºC

K

Extrapolated onset of endotherms

Extrapolated onset of decomposition

164.37

438

 Thermographic Data – Determination 2

Thermal Event

Interpretation

Temperature

ºC

K

Extrapolated onset of endotherms

Extrapolated onset of decomposition

165.15

438

Atmospheric pressure: 99.21 kPa

Overall decomposition temperature: From approximately 438 K

 

SEE ATTACHMENT FOR THERMOGRAMS

Applicant's summary and conclusion

Conclusions:
Sulfoclor LF 1013 has been determined to decompose from approximately 438 K at 99.21 kPa. As Sulfoclor LF 1013 decomposed, no value for boiling temperature could be determined experimentally.
Executive summary:

Boiling Temperature. 

Sulfoclor LF 1013 has been determined to decompose from approximately 438 K at 99.21 kPa, by differential scanning caloritry, using ASTM E537-86, designed to be compatible with Method A2 Boiling Temperature of Commission Regulation (EC) No 440/2008 of 30 May 2008. 

As Sulfoclor LF 1013 decomposed, no value for boiling temperature could be determined experimentally.