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The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
flash point of flammable liquids
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Testing was conducted between 15 April 2010 and 07 May 2010.
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: see 'Remark'
Remarks:
Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results. The study report was conclusive, done to a valid guideline and the study was conducted under GLP conditions.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2010
Report date:
2010

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.9 (Flash-Point)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
equilibrium method closed cup

Test material

Constituent 1
Reference substance name:
SULFOCLOR LF 1013
IUPAC Name:
SULFOCLOR LF 1013
Constituent 2
Reference substance name:
Paraffin waxes and Hydrocarbon waxes, chloro, sulfochlorinated
EC Number:
269-145-7
EC Name:
Paraffin waxes and Hydrocarbon waxes, chloro, sulfochlorinated
Cas Number:
68188-19-2
Molecular formula:
CnHxCly(SO2Cl)z n= 14 - 17 or n=17 - 30 ; x=2n+2-y-z
IUPAC Name:
Paraffin waxes and Hydrocarbon waxes, chloro, sulfochlorinated
Details on test material:
Sponsor's identification: SULFOCLOR LF 1013
CAS No : 68188-19-2
Description : pale yellow slightly viscous liquid
Purity : >99%
Batch number: None supplied
Label : Sulfoclor LF 1013 TANQUE 25.09.2009
Date received: 05 February 2010
Expiry date : 23 September 2010
Storage conditions: room temperature in the dark

Results and discussion

Flash point
Remarks on result:
other: Sulfoclor LF 1013 has been determined not to have a flash point below its boiling temperature.

Any other information on results incl. tables

                     

  Results

Temperature (ºC)

Observations

22.0

No flash.

27.0

No flash.

32.0

No flash.

37.0

No flash.

42.0

No flash.

47.0

No flash.

52.0

No flash.

57.0

No flash.

62.0

No flash.

67.0

No flash.

72.0

No flash.

72.0(fresh sample)

No flash.

77.0

No flash.

82.0

No flash.

87.0

No flash.

92.0

No flash.

97.0

No flash.

102.0(fresh sample)

No flash.

107.0

No flash.

112.0

No flash.

117.0

No flash.

122.0

No flash.

127.0

No flash.

132.0

No flash.

137.0

No flash.

142.0

No flash.

147.0

No flash.

152.0

No flash.

152.0(fresh sample)

No flash.

157.0

No flash.

162.0

No flash.

167.0

No flash, the sample was boiling.

162.0(fresh sample)

No flash, the sample was boiling.

152.0(fresh sample)

No flash, the sample was not boiling.

154.0

No flash, the sample was not boiling.

156.0

No flash, the sample was not boiling.

158.0

No flash, the sample was not boiling.

159.0

No flash, the sample was boiling.

159.0(fresh sample)

No flash, the sample was boiling.

157.0(fresh sample)

No flash, the sample was not boiling.

157.0(fresh sample)

No flash, the sample was not boiling.

159.0(fresh sample)

No flash, the sample was boiling.

Applicant's summary and conclusion

Conclusions:
Sulfoclor LF 1013 has been determined not to have a flash point below its boiling temperature.
Executive summary:
The flash point was determined using a closed cup equilibrium method. The method was designed to be compatible with Method A9 Flash Point of CommissionRegulation (EC) No 440/2008 of 30 May 2008. An aliquot (2 ml for temperatures up to 100ºC and 4 ml for temperatures above 100ºC) of the test item was injected into the sample cup of the Setaflash 30000.0 tester. The sample was heated and allowed to equilibrate at the set temperature. The test flame was introduced into the sample cup for approximately 2½ seconds by sliding the cup shutter open. Observations were made for ignition of the vapour. If no ignition occurred, the temperature was increased and the test flame re-introduced. This was repeated until the lowest reproducible temperature at which a flash occurred, using a fresh sample, was determined, or until the sample boiled. Sulfoclor LF 1013 has been determined not to have a flash point below its boiling temperature.