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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2016-12-05
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018
Report date:
2018

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
27. July 1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
31. May 2008
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
capillary method

Test material

Constituent 1
Chemical structure
Reference substance name:
2,2'-[[3-chloro-4-[[4-[[2-(sulphooxy)ethyl]sulphonyl]phenyl]azo]phenyl]imino]bisethyl bis(hydrogen sulphate), potassium sodium salt
EC Number:
287-719-5
EC Name:
2,2'-[[3-chloro-4-[[4-[[2-(sulphooxy)ethyl]sulphonyl]phenyl]azo]phenyl]imino]bisethyl bis(hydrogen sulphate), potassium sodium salt
Cas Number:
85567-07-3
Molecular formula:
C36H42Cl2KN6NaO28S8
IUPAC Name:
2,2'-[[3-chloro-4-[[4-[[2-(sulphooxy)ethyl]sulphonyl]phenyl]azo]phenyl]imino]bisethyl bis(hydrogen sulphate), potassium sodium salt
Test material form:
solid
Details on test material:
Batch: 1283067001

Results and discussion

Melting / freezing point
Key result
Decomposition:
yes
Decomp. temp.:
ca. 210 °C
Remarks on result:
not determinable

Any other information on results incl. tables

Preliminary test: At about 210 °C the test item started to turn black and decomposed. No melting point was observed.

Applicant's summary and conclusion

Conclusions:
At about 210 °C the test item started to turn black and decomposed. No melting point was observed.
Executive summary:

The test was carried out according to OECD guideline 102 and EC method A.1. Capillary tubes filled with the test item were heated in a metal block. The test item started to decompose at about 210 °C, hence no melting point could be observed.