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Physical & Chemical properties

Particle size distribution (Granulometry)

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Reference
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2017
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
guideline study without detailed documentation
Qualifier:
according to guideline
Guideline:
ISO 13320 (Particle size analysis - Laser diffraction methods)
Deviations:
not specified
GLP compliance:
no
Type of method:
Laser scattering/diffraction
Type of particle tested:
primary particle
Type of distribution:
volumetric distribution
Specific details on test material used for the study:
400 mesh material as sold
Lot 702M130
Key result
Percentile:
D50
Mean:
11.65 µm
Remarks on result:
other: standard deviation not reported
Percentile:
other: D97
Mean:
30.82 µm
Remarks on result:
other: standard deviation not reported
Percentile:
other: D6
Mean:
0.539 µm
Remarks on result:
other: standard deviation not reported
Percentile:
other: D5
Mean:
0.43 µm
Remarks on result:
other: standard deviation not reported
Conclusions:
The median particle size (D50) of a typical technical grade calcium hexaboride powder is appr. 12 µm, the D97 is appr. 31 µm.
Executive summary:

The median particle size (D50) of a typical technical grade calcium hexaboride powder is appr. 12 µm, the D97 is appr. 31 µm. The study was conducted by laser diffraction in an automated instrument according to a guideline method but without detailed documentation and not under GLP. The study is therefore considered reliable with restrictions.

Description of key information

The median particle size (D50) of a typical technical grade calcium hexaboride powder is appr. 12 μm, the D97 is appr. 31 μm.

Additional information

The study was conducted by laser diffraction in an automated instrument according to a guideline method but without detailed documentation and not under GLP. The study is therefore considered reliable with restrictions.