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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Principles of method if other than guideline:
The amine oxides were synthesised by oxidation of the corresponding trialkylamine with H2O2. After oxidation and isolation the products were thoroughly dried by azeotropic distillation with benzene and toluene followed by multiple crystallisations (4-5 times) from dry Me2CO and dried over P4O10 in a high vacuum. The purity was checked by TLC and IR spectra.
GLP compliance:
no
Type of method:
other: method not specified, however a capllary method was used for shorter chain length amine oxides
Melting / freezing pt.:
130 - 134 °C
Atm. press.:
1 013 hPa
Remarks on result:
other: C12 AO

A study is described in the literature [Devinsky et al 1985] where the authors measured the melting points of several pure alkyl dimethylamine oxide from C10 to C16. The measured melting point for C12 AO was 130 - 134°C.

Conclusions:
The melting point of the substance is approximately 130 -134 deg C.

Description of key information

The melting point is in the range of 130-134 °C

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
130 °C

Additional information

The melting point of C12 AO is in the range 130 -134 °C [Devinsky et al 1985].