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Diss Factsheets

Physical & Chemical properties

Particle size distribution (Granulometry)

Administrative data

Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
12. 08. 2021
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2021
Report date:
2021

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
ISO 13320 (Particle size analysis - Laser diffraction methods)
Version / remarks:
First edition 2009-10-01, Corrected version 2009-12-01
Deviations:
no
Qualifier:
according to guideline
Guideline:
other: Guidance Document on the Determination of Particle Size Distribution, Fibre Length and Diameter Distribution of Chemical Substances EUR 20268 EN
Version / remarks:
2002
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
Laser scattering/diffraction
Type of particle tested:
primary particle
Type of distribution:
volumetric distribution

Test material

Constituent 1
Chemical structure
Reference substance name:
4H-1,2,4-triazol-4-ylamine
EC Number:
209-533-5
EC Name:
4H-1,2,4-triazol-4-ylamine
Cas Number:
584-13-4
Molecular formula:
C2H4N4
IUPAC Name:
4H-1,2,4-triazol-4-ylamine
Test material form:
solid

Results and discussion

Particle sizeopen allclose all
Key result
Percentile:
D50
Mean:
756.52 µm
St. dev.:
99.27
Percentile:
D10
Mean:
502.86 µm
St. dev.:
96.66
Percentile:
D90
Mean:
1 064.02 µm
St. dev.:
210.59

Applicant's summary and conclusion

Conclusions:
The particle size distribution of the test item, 4H-1,2,4-triazol-4-amine, was determined. The laser diffraction method was used.
Particle size distribution of test item, 4H-1,2,4-triazol-4-amine, is characterized by the following table:

Median(µm) Diameter on Cumul. 10% (µm) Diameter on Cumul. 90% (µm) Span (-)
Final result 756.52 502.86 1064.02 0.74
Ext. uncert. 99.27 96.66 210.59 -

Extended uncertainty was calculated from standard deviation using coefficient of 2.
Executive summary:

The particle size distribution of the test item, 4H-1,2,4-triazol-4-amine, was determined. The laser diffraction method was used.


The procedure was performed according to Standard ISO 13320:2009 Particle size analysis – Laser diffraction methods, First edition 2009-10-01 and with the considering of the recommendation of Guidance Document on the Determination of Particle Size Distribution, Fibre Length and Diameter Distribution of Chemical Substances, EUR 20268 EN (2002).


Particle size distribution of test item, 4H-1,2,4-triazol-4-amine, is characterized by the following table:



























 



Median


(µm)



Diameter on Cumulative 10%


(µm)



Diameter on Cumulative 90%


(µm)



Span


(-)



Final result



756.52



502.86



1064.02



0.74



Extended uncertainty



99.27



96.66



210.59



-



Extended uncertainty was calculated from standard deviation using coefficient of 2.