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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
supporting study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: According to OECD guidline 103.
Cross-reference
Reason / purpose for cross-reference:
reference to same study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2006
Report date:
2006

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Deviations:
no
Remarks:
The study was conducted according to the guideline in effect at time of study conduct.
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
Remarks:
The study was conducted according to the guideline in effect at time of study conduct.
GLP compliance:
yes (incl. QA statement)
Type of method:
method according to Siwoloboff

Test material

Constituent 1
Chemical structure
Reference substance name:
-
EC Number:
481-150-8
EC Name:
-
Cas Number:
500011-86-9
Molecular formula:
C9H5BrClN3O2
IUPAC Name:
3-bromo-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxylic acid
Constituent 2
Reference substance name:
DBC80
IUPAC Name:
DBC80
Constituent 3
Reference substance name:
1H-Pyrazole-5-Carboxylic Acid, 3-Bromo-1-(3-Chloro-2-Pyridinyl)-
IUPAC Name:
1H-Pyrazole-5-Carboxylic Acid, 3-Bromo-1-(3-Chloro-2-Pyridinyl)-
Details on test material:
- Name of test material (as cited in study report): IN-DBC80
- Molecular weight (if other than submission substance): 302.52
- Physical state: Tan colour powder
- Analytical purity: 96.7%
- Lot/batch No.: 008
- Expiration date of the lot/batch: 22nd July, 2008
- Storage condition of test material: Stored in the dark at room temperature.

Results and discussion

Boiling point
Decomposition:
yes
Decomp. temp.:
208 - 210 °C
Remarks on result:
other: The preliminary test indicated that IN-DBC80 was decomposed at 208°C.

Any other information on results incl. tables

Decomposition Point Determination for IN-DBC80

Replicate Decomposition Point (deg C)* Decomposition Point (K)*
1 208 - 210 481.15 - 483.15
2 208 - 210 481.15 - 483.15
3 208 - 210 481.15 - 483.15
Mean 208 - 210 481.15 - 483.15

* - Remarks: IN-DBC80 decomposed prior to reaching a boiling point.

Applicant's summary and conclusion

Conclusions:
Under the conditions of this study, IN-DBC80 decomposed prior to reaching a boiling point. IN-DBC80 decomposed at 208 - 210 degrees Celcius.