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Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2018-05-28 to 2018-07-18
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
1995
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Qualifier:
according to guideline
Guideline:
other: •EPA OCSPP Test Guideline 830.7200: Melting Point / Melting Range
Version / remarks:
1998
Qualifier:
according to guideline
Guideline:
other: CIPAC MT 1: Freezing Point
Version / remarks:
2009
GLP compliance:
no
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
SOURCE OF TEST MATERIAL
- Source and lot/batch No.of test material:
R-127 / batch no. 180131
- Expiration date of the lot/batch:
2019-01-31

STABILITY AND STORAGE CONDITIONS OF TEST MATERIAL
- Storage condition of test material:
Dry and dark at ambient temperature (10 – 30 °C)
- Stability under test conditions:
stable

TREATMENT OF TEST MATERIAL PRIOR TO TESTING
- Treatment of test material prior to testing:
none
Key result
Melting / freezing pt.:
>= -75 - <= -72 °C
Atm. press.:
>= 1 000 - <= 1 005 hPa
Decomposition:
no
Sublimation:
no
Conclusions:
The test item diethyl sulphate, compound with 2-(heptadec-8-enyl)-4,5-dihydro-1H-imidazole-1-ethanol (1:1) has a melting range of -75 to -72 °C at atmospheric pressure (1000 – 1005 hPa) as determined by differential scanning calorimetry and test tube according to Regulation EC No. 440/2008 Method A.1. and OECD Test Guideline 102 (1995).
Executive summary:

The melting point of diethylsulphate, compound with 2 -(heptadec-8 -enyl)-4,5 -dihydro-1H-imidazole-1 -ethanol (1:1) was determined ina guideline study.

The test item diethylsulphate, compound with 2 -(heptadec-8 -enyl)-4,5 -dihydro-1H-imidazole-1 -ethanol (1:1) has amelting rangeof -75 to -72 °C at atmospheric pressure (1000 – 1005 hPa) as determined by differential scanning calorimetry and test tube according to Regulation EC No. 440/2008 Method A.1. and OECD Test Guideline 102 (1995).

Description of key information

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-72 °C

Additional information