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Physical & Chemical properties

Particle size distribution (Granulometry)

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Administrative data

Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
From 2017-03-23 to 2017-03-23
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2017
Report date:
2017

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 110 (Particle Size Distribution / Fibre Length and Diameter Distributions - Method A: Particle Size Distribution (effective hydrodynamic radius)
Deviations:
no
Qualifier:
according to guideline
Guideline:
other: NF ISO 2591-1
Version / remarks:
1989
Deviations:
yes
Remarks:
For particle size distribution test; the loss of test item was 5.6% which is higher than 2% (see NF ISO 2591-1 (1989)). This deviation was not considered to have affected the quality or the interpretation of the results obtained.
Qualifier:
according to guideline
Guideline:
other: NF X11-507
Version / remarks:
1989
GLP compliance:
yes (incl. QA statement)
Type of method:
sieving
Type of particle tested:
primary particle
Type of distribution:
volumetric distribution

Test material

1
Chemical structure
Reference substance name:
Copper, [29H,31H-phthalocyaninato(2-)-N29,N30,N31,N32]-, [[3-(cyclohexylamino)propyl]amino]sulfonyl derivs.
EC Number:
309-627-7
EC Name:
Copper, [29H,31H-phthalocyaninato(2-)-N29,N30,N31,N32]-, [[3-(cyclohexylamino)propyl]amino]sulfonyl derivs.
Cas Number:
100545-46-8
Molecular formula:
C32H16-τN8Cu.(SO3)m.(SO3H)p.(C9H19N2SO2)O.(C9H20N2SO2)n
IUPAC Name:
Copper, [29H,31H-phthalocyaninato(2-)-N29,N30,N31,N32]-, [[3-(cyclohexylamino)propyl]amino]sulfonyl derivs.
Test material form:
solid: particulate/powder
Specific details on test material used for the study:
STORAGE CONDITIONS OF TEST MATERIAL
- Storage condition of test material: in darkness at room temperature


Results and discussion

Particle size distribution at different passagesopen allclose all
No.:
#1
Size:
ca. 25 µm
Distribution:
ca. 24.1 %
Remarks on result:
other: cumulated undersized particles
No.:
#2
Size:
ca. 32 µm
Distribution:
ca. 33.9 %
Remarks on result:
other: cumulated undersized particles
No.:
#3
Size:
ca. 45 µm
Distribution:
ca. 82.3 %
Remarks on result:
other: cumulated undersized particles
No.:
#4
Size:
ca. 63 µm
Distribution:
ca. 87.7 %
Remarks on result:
other: cumulated undersized particles
No.:
#5
Size:
ca. 90 µm
Distribution:
ca. 91.8 %
Remarks on result:
other: cumulated undersized particles
No.:
#6
Size:
ca. 125 µm
Distribution:
ca. 95.6 %
Remarks on result:
other: cumulated undersized particles
No.:
#7
Size:
ca. 180 µm
Distribution:
ca. 97.9 %
Remarks on result:
other: cumulated undersized particles
No.:
#8
Size:
ca. 250 µm
Distribution:
ca. 99.2 %
Remarks on result:
other: cumulated undersized particles
No.:
#9
Size:
ca. 355 µm
Distribution:
ca. 99.7 %
Remarks on result:
other: cumulated undersized particles
No.:
#10
Size:
ca. 500 µm
Distribution:
ca. 99.8 %
Remarks on result:
other: cumulated undersized particles
Size:
ca. 710 µm
Distribution:
ca. 99.9 %
Remarks on result:
other: cumulated undersized particles

Any other information on results incl. tables

Results

Ambient humidity About 38%

Temperature About 20 °C

Mass of test item used 30.00 g

The loss of test item represented 5.6% of the total quantity.

Applicant's summary and conclusion

Conclusions:
After the test, it was shown that the majority of the particles (82.3%) had a size lower than 45 μm. Due to the thickness of the powder, a significative quantity of powder (5.6%)
was lost.
Executive summary:

The test was performed according to OECD Guideline No. 110 (1981), NF ISO 2591 -1 (1989) and NF X11 -507 (1989)

 

The majority of the particles (82.3%) had a size lower than 45 μm. Due to the thickness of the powder, a significative quantity of powder (5.6%) was lost.