Registration Dossier
Registration Dossier
Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.
The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.
Use of this information is subject to copyright laws and may require the permission of the owner of the information, as described in the ECHA Legal Notice.
EC number: 813-543-0 | CAS number: 73984-93-7
Boiling point
Administrative data
- Endpoint:
- boiling point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- Experimental starting date: 20 October 2017 Experimental completion date: 17 November 2017
- Reliability:
- 1 (reliable without restriction)
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 018
Materials and methods
Test guidelineopen allclose all
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.2 (Boiling Temperature)
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 103 (Boiling Point)
- GLP compliance:
- yes
- Type of method:
- differential scanning calorimetry
Test material
- Reference substance name:
- 1,3,4-Thiadiazole-2(3H)-thione, 5-(tert-dodecyldithio)-
- EC Number:
- 813-543-0
- Cas Number:
- 73984-93-7
- Molecular formula:
- C14H26N2S4
- IUPAC Name:
- 1,3,4-Thiadiazole-2(3H)-thione, 5-(tert-dodecyldithio)-
- Test material form:
- liquid
- Details on test material:
- - Storage: in a sealed container at room temperature
Constituent 1
- Specific details on test material used for the study:
- Information as provided by the Sponsor. The Certificate of Analysis provided by the Sponsor is attached (Please see Attachment Section of this Summary).
Identification: A-153
Appearance/Physical state: pale yellow viscous liquid
Batch: B16001086
Purity: UVCB Substance (treat as 100%)
Expiry date: 01 March 2018
Storage conditions: room temperature, in the dark
Results and discussion
Boiling point
- Key result
- Boiling pt.:
- ca. 519 K
- Atm. press.:
- 101.3 kPa
- Decomposition:
- ambiguous
Any other information on results incl. tables
Results
The thermographic data for determinations 1 and 2 are shown in the following table. The thermograms for determinations 1 and 2 are shown in the Attachment Section of this Summary.
Thermographic Data
Thermal Event |
Interpretation |
Temperature |
|||
Determination 1 |
Determination 2 |
||||
ºC |
K |
ºC |
K |
||
Endotherm |
Phase transition - boiling |
245.4 |
518.6 |
245.8 |
519.0 |
Atmospheric pressure: 101.3 kPa
After heating to 450 °C, the samples had lost approximately 98% of their original mass.
Boiling point: Mean Boiling Temperature: 245.6 ± 0.5 °C (518.8 ± 0.5 K)
Applicant's summary and conclusion
- Conclusions:
- The boiling temperature of the test item was determined to be 246 ± 0.5 °C (519 ± 0.5 K) at 101.3 kPa.
- Executive summary:
The determination was carried out by differential scanning calorimetry, using a procedure designed to be compatible with Method A.2 Boiling Temperature of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 103 of the OECD Guidelines for Testing of Chemicals, 27 July 1995 and Method 830.7220 of the OCSPP Guidelines, August 1996.
Conclusion
The boiling temperature of the test item was determined to be 246 ± 0.5 °C (519 ± 0.5 K) at 101.3 kPa.
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
Reproduction or further distribution of this information may be subject to copyright protection. Use of the information without obtaining the permission from the owner(s) of the respective information might violate the rights of the owner.
