Registration Dossier
Registration Dossier
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EC number: 269-119-5 | CAS number: 68187-67-7
Auto flammability
Administrative data
- Endpoint:
- auto-ignition temperature (liquids)
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- The study was conducted between 26 October 2014 and 02 December 2014
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
- Remarks:
- GLP guideline study
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 015
- Report date:
- 2015
Materials and methods
Test guideline
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.15 (Auto-Ignition Temperature (Liquids and Gases))
- Deviations:
- no
- GLP compliance:
- yes (incl. QA statement)
Test material
- Reference substance name:
- Amines, C12-14-tert-alkyl, isooctyl mono phosphates
- IUPAC Name:
- Amines, C12-14-tert-alkyl, isooctyl mono phosphates
- Reference substance name:
- Unknown, including minor amounts of diphosphate species, water. Possibly residual unreacted starting material and unknown byproducts.
- IUPAC Name:
- Unknown, including minor amounts of diphosphate species, water. Possibly residual unreacted starting material and unknown byproducts.
- Test material form:
- liquid: viscous
Constituent 1
Constituent 2
Results and discussion
Auto-ignition temperature (liquids / gases)
- Key result
- Auto-ignition temperature:
- >= 281 - <= 291 °C
- Atm. press.:
- >= 100.9 - <= 102.2 kPa
Any other information on results incl. tables
Results of the auto-ignition temperature determination are shown in the following table.
Test Temperature (ºC) |
Test Volume (µL) |
Ignition Delay (s) |
Observations |
200 (clean flask) |
70 |
>300 |
No ignition. Grey fumes were emitted. |
250 (clean flask) |
70 |
>300 |
No ignition. Grey fumes were emitted. |
300 (clean flask) |
70 |
>300 |
No ignition. Grey fumes were emitted. |
350 |
70 |
5 |
A yellow flame. Grey fumes were emitted. |
340 (clean flask) |
70 |
>300 |
No ignition. Grey fumes were emitted. |
346 (clean flask) |
70 |
7 |
A yellow flame. Grey fumes were emitted. |
344 (clean flask) |
70 |
>300 |
No ignition. Grey fumes were emitted. |
344 (clean flask) |
200 |
4 |
A yellow flame. Grey fumes were emitted. |
342 (clean flask) |
200 |
3 |
A yellow flame. Grey fumes were emitted. |
340 (clean flask) |
200 |
4 |
A yellow flame. Grey fumes were emitted. |
338 (clean flask) |
200 |
6 |
A yellow flame. Grey fumes were emitted. |
336 (clean flask) |
200 |
8 |
A yellow flame. Grey fumes were emitted. |
334 (clean flask) |
200 |
8 |
A yellow flame. Grey fumes were emitted. |
330 (clean flask) |
200 |
9 |
A yellow flame. Grey fumes were emitted. |
320 (clean flask) |
200 |
8 |
A yellow flame. Grey fumes were emitted. |
310 (clean flask) |
200 |
>300 |
No ignition. Grey fumes were emitted. |
316 (clean flask) |
200 |
>300 |
No ignition. Grey fumes were emitted. |
318 (clean flask) |
200 |
10 |
A yellow flame. Grey fumes were emitted. |
316 (clean flask) |
400 |
8 |
A yellow/blue flame. Grey fumes were emitted. |
314 (clean flask) |
400 |
10 |
A yellow/blue flame. Grey fumes were emitted. |
312 (clean flask) |
400 |
11 |
A yellow/blue flame. Grey fumes were emitted. |
310 (clean flask) |
400 |
>300 |
No ignition. Grey fumes were emitted. |
310 (clean flask) |
600 |
10 |
A yellow/blue flame. Grey fumes were emitted. |
308 (clean flask) |
600 |
10 |
A yellow/blue flame. Grey fumes were emitted. |
306 (clean flask) |
600 |
11 |
A yellow/blue flame. Grey fumes were emitted. |
304 (clean flask) |
600 |
16 |
A yellow/blue flame. Grey fumes were emitted. |
Test Temperature (ºC) |
Test Volume (µL) |
Ignition Delay (s) |
Observations |
302 (clean flask) |
600 |
15 |
A yellow/blue flame. Grey fumes were emitted. |
300 (clean flask) |
600 |
18 |
A yellow/blue flame. Grey fumes were emitted. |
298 (clean flask) |
600 |
19 |
A yellow/blue flame. Grey fumes were emitted. |
296 (clean flask) |
600 |
18 |
A yellow/blue flame. Grey fumes were emitted. |
294 (clean flask) |
600 |
>300 |
No ignition. Grey fumes were emitted. |
294 (clean flask) |
800 |
24 |
A yellow/blue flame. Grey fumes were emitted. |
292 (clean flask) |
800 |
27 |
A yellow/blue flame. Grey fumes were emitted. |
290 (clean flask) |
800 |
29 |
A yellow/blue flame. Grey fumes were emitted. |
288 (clean flask) |
800 |
33 |
A yellow/blue flame. Grey fumes were emitted. |
286 (clean flask) |
800 |
33 |
A yellow/blue flame. Grey fumes were emitted. |
284 (clean flask) |
800 |
>300 |
No ignition. Grey fumes were emitted. |
284 (clean flask) |
1000 |
>300 |
No ignition. Grey fumes were emitted. |
284 (clean flask) |
1200 |
>300 |
No ignition. Grey fumes were emitted. |
284 (clean flask) |
1400 |
>300 |
No ignition. Grey fumes were emitted. |
284 (clean flask) |
1600 |
>300 |
No ignition. Grey fumes were emitted. |
Room temperature: 20 to 21 °C
Atmospheric pressure: 100.9 to 102.2 kPa
Applicant's summary and conclusion
- Conclusions:
- The test item has been determined to have an auto-ignition temperature of 286 ± 5 °C.
- Executive summary:
The auto-ignition temperature (liquids and gases) was 286 ± 5 °C, using a procedure designed to be compatible with Method A15 Auto-Ignition Temperature (Liquids and Gases) of Commission Regulation (EC) No 440/2008 of 30 May 2008.
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