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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
21.11.2018 to 04.03.2019
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018
Report date:
2019

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
[2,2,6,6-tetramethyl-4-(trimethylazaniumyl)piperidin-1-yl]oxidanyl chloride
EC Number:
814-375-0
Cas Number:
67036-09-3
Molecular formula:
C12H26N2OCl
IUPAC Name:
[2,2,6,6-tetramethyl-4-(trimethylazaniumyl)piperidin-1-yl]oxidanyl chloride
Test material form:
solid

Results and discussion

Boiling point
Key result
Decomposition:
yes
Decomp. temp.:
>= 253 - <= 270 °C
Remarks on result:
other:
Remarks:
Two mass loss steps were registered at approx. 253 °C with a mass loss of 45.4 % and at approx. 270 °C with a mass loss of 49.5 % (0.3 % mass loss due to purging). A further small peak could be observed at approx. 289 °C. After cooling the residue inside the crucible looked like anthracite and had shrunk strongly. The course of the curve showed no indication for a pure boiling behaviour but for decomposition.

Applicant's summary and conclusion

Conclusions:
The boiling temperature of the test item was determined by differential scanning calorimetry
according to OECD Test Guideline 103 [adopted on 27 July 1995] and EU test method A.2 "Boiling
temperature", Council Regulation (EC) No 440/2008 of 30 May 2008.
Boiling temperature: no boiling; decomposition