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Physical & Chemical properties

Particle size distribution (Granulometry)

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Reference
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
18 May 1993 and 1 October 1993
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Qualifier:
according to guideline
Guideline:
other: Method DIN 5374.
Deviations:
not specified
GLP compliance:
yes (incl. QA statement)
Type of method:
sieving
Remarks:
air-jet sieve method
Type of particle tested:
primary particle
Type of distribution:
mass based distribution
Specific details on test material used for the study:
No further details specified in the study report.
Remarks on result:
not measured/tested
Key result
Remarks on result:
other: Percentile not determined in the test
No.:
#1
Size:
10 µm
Distribution:
0 %
No.:
#2
Size:
45 µm
Distribution:
16.3 %
No.:
#3
Size:
75 µm
Distribution:
19.4 %
No.:
#4
Size:
125 µm
Distribution:
32.7 %
No.:
#5
Size:
250 µm
Distribution:
58.2 %
No.:
#6
Size:
355 µm
Distribution:
80.6 %
No.:
#7
Size:
425 µm
Distribution:
88.3 %

The weight of test material retained on each sieve is given below:

Sieve aperture size (μm)

Air-jet pressure (kPa)

Weight of test material transferred to sieve (g)

Weight of test material retained by sieve (g)

10

45

75

125

250

355

425

11.5 – 12.5

5.2 – 5.7

5.2 – 5.7

5.2 – 5.7

5.2 – 5.7

5.2 – 5.7

5.2 – 5.7

2.0

19.6

15.9

15.2

12.6

7.5

3.0

2.0

16.4

15.3

12.6

7.6

3.1

1.5

 

Sieve aperture size (μm)

Weight of test material passed through sieve (g)

% test material having particle size less than sieve aperture size

10

45

75

125

250

355

425

0.0

3.2

0.6

2.6

5.0

4.4

1.5

0

16.3

19.4

32.7

58.2

80.6

88.3

 

Conclusions:
The particle size distribution of JPR BLUE 100 (Lot Number 303001) in the range 10 to 425 μm was determined and the results are detailed below:
Particle size (μm) % test material having less than particle size indicated
10 0
45 16.3
75 19.4
125 32.7
250 58.2
355 80.6
425 88.3
Executive summary:

A number of general physico-chemical properties of the compound JPR BLUE 100 (Lot Number 303001) have been determined at the request of the sponsor.

 

The particle size distribution was determined using the air-jet sieve method, based on DIN 5374.

 

The particle size distribution of JPR BLUE 100 (Lot Number 303001) in the range 10 to 425 μm was determined and the results are detailed below:

Particle size (μm)       % test material having less than particle size indicated

10                               0

45                               16.3

75                               19.4

125                             32.7

250                             58.2

355                             80.6

425                             88.3

Description of key information

The particle size distribution of JPR BLUE 100 (Lot Number 303001) in the range 10 to 425 μm was determined and the results are detailed below:

Particle size(μm)       % test material having less than particle size indicated

10                               0

425                             88.3

Additional information

A number of general physico-chemical properties of the compound JPR BLUE 100 (Lot Number 303001) have been determined at the request of the sponsor.

The particle size distribution was determined using the air-jet sieve method, based on DIN 5374.

The particle size distribution of JPR BLUE 100 (Lot Number 303001) in the range 10 to 425 μm was determined and the results are detailed below:

Particle size(μm)       % test material having less than particle size indicated

10                               0

45                               16.3

75                               19.4

125                             32.7

250                             58.2

355                             80.6

425                             88.3