Oleic acid, compound with 2-amino-2-methylpropan-1-ol (1:1)

Auto flammability

Administrative data

Endpoint:

auto-ignition temperature (liquids)

Type of information:

experimental study

Adequacy of study:

key study

Study period:

Experimental starting date: 14 August 2017 Experimental completion date: 18 September 2017

Reliability:

1 (reliable without restriction)

Data source

Reference

Reference Type:

study report

Title:

Unnamed

Year:

2017

Report date:

2017

Materials and methods

Test guideline

Qualifier:

according to guideline

Guideline:

EU Method A.15 (Auto-Ignition Temperature (Liquids and Gases))

Deviations:

no

GLP compliance:

yes

Test material

Test material information

Constituent 1

Reference substance name:

Oleic acid, compound with 2-amino-2-methylpropan-1-ol (1:1)

EC Number:

268-793-8

EC Name:

Oleic acid, compound with 2-amino-2-methylpropan-1-ol (1:1)

Cas Number:

68140-41-0

Molecular formula:

C18H34O2.C4H11NO

IUPAC Name:

oleic acid, compound with 2-amino-2-methylpropan-1-ol (1:1)

Specific details on test material used for the study:

Information as provided by the Sponsor. The Certificate of Analysis provided by the Sponsor is presented as Annex 1 (Please see attachment section of this summary)

Identification: Oleic AMP
CAS No: 68140-41-0
Structure: Please see illustration section below.
Appearance/Physical state: Yellow paste
Batch: LAB4436
Purity: 100%
Expiry date: 21 February 2018
Storage conditions: Room temperature in the dark

Results and discussion

Auto-ignition temperature (liquids / gases)

Key result

Auto-ignition temperature:

260 °C

Atm. press.:

101.7 kPa

Any other information on results incl. tables

Results

Results of the auto-ignition temperaturedetermination are shown in the following table:

Test Temperature (ºC)	Clean Flask (Yes/No)	Weight	Ignition Delay (s)	Observations
200	Yes	0.3	>300	No ignition. Grey fumes were emitted.
250	Yes	0.2	>300	No ignition. Grey fumes were emitted.
300	Yes	0.2	52	A yellow/orange flame. Grey fumes were emitted.
280	No	0.2	92	A red/orange flame. Grey fumes were emitted.
270	No	0.3	109	An orange flame. Grey fumes were emitted.
260	No	0.2	175	A red/orange flame. Grey fumes were emitted.
258	No	0.3	>300	No ignition. Grey fumes were emitted.
258	Yes	0.3	>300	No ignition. Grey fumes were emitted.
258	Yes	0.5	>300	No ignition. Grey fumes were emitted.

258	Yes	0.6	>300	No ignition. Grey fumes were emitted.
258	Yes	0.8	>300	No ignition. Grey fumes were emitted.
258	Yes	1.0	>300	No ignition. Grey fumes were emitted.

Applicant's summary and conclusion

Conclusions:

The test item has been determined to have an auto-ignition temperature of 260 ± 5 °C.

Executive summary:

The determination was carried out using a procedure*designed to be compatible with Method A.15 Auto-IgnitionTemperature (Liquids and Gases) of Commission Regulation (EC) No 440/2008 of 30 May 2008.

Apparatus:      Carbolite flask heater

*Based on, Anon (1987), Electrical Apparatus for Explosive Gas Atmospheres. Part 4: Method of Test for Ignition Temperature. IEC Publications79-4,P1-19.

Conclusion

The test item has been determined to have an auto-ignition temperature of 260 ± 5 °C.

NOTE: Any of data in this dataset are disseminated by the European Union on a right-to-know basis and this is not a publication in the same sense as a book or an article in a journal. The right of ownership in any part of this information is reserved by the data owner(s). The use of this information for any other, e.g. commercial purpose is strictly reserved to the data owners and those persons or legal entities having paid the respective access fee for the intended purpose.