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Physical & Chemical properties

Particle size distribution (Granulometry)

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Reference
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Not stated
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
comparable to guideline study with acceptable restrictions
Qualifier:
no guideline followed
Principles of method if other than guideline:
Particle size investigated using laser diffraction technology.
GLP compliance:
not specified
Type of method:
Laser scattering/diffraction
Percentile:
D10
Mean:
0.2 µm
Remarks on result:
other: standard deviation information not provided
Percentile:
D50
Mean:
2.1 µm
Remarks on result:
other: standard deviation information not provided
Percentile:
D90
Mean:
6.7 µm
Remarks on result:
other: standard deviation information not provided
Conclusions:
Under the conditions of this study the D50 was 2.1 µm, D10 was 0.2 µm and D90 was 6.7 µm.
Executive summary:

The analysis was carried out on a Microtrac S3500 which uses laser diffraction technology. An amount of detergent (TSPP 5 %) was added to improve the distribution of the material in the solvent distilled water. The suspension of the material was treated ultrasonically to destroy potential agglomerates. Particle size determination was conducted in triplicate and the average taken.

Under the conditions of this study the D50 was 2.1 µm, D10 was 0.2 µm and D90 was 6.7 µm.

Description of key information

Under the conditions of this study the D50 was 2.1 µm, D10 was 0.2 µm and D90 was 6.7 µm.

Additional information

The particle size distribution of the test material was investigated with a Microtrac S3500 which uses laser diffraction technology. An amount of detergent (TSPP 5 %) was added to improve the distribution of the material in the solvent distilled water. The suspension of the material was treated ultrasonically to destroy potential agglomerates. Particle size determination was conducted in triplicate and the average taken.

Under the conditions of this study the D50 was 2.1 µm, D10 was 0.2 µm and D90 was 6.7 µm.