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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
water solubility
Type of information:
experimental study
Adequacy of study:
key study
Study period:
29 October 1996 - 12 February 1997
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: EC Directive 92/69 Annex V mrthod A.6 OECD Guideline 105 (1995)
Cross-reference
Reason / purpose for cross-reference:
reference to same study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
1997
Report date:
1997

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.6 (Water Solubility)
Qualifier:
according to guideline
Guideline:
OECD Guideline 105 (Water Solubility)
GLP compliance:
yes (incl. QA statement)
Type of method:
flask method

Test material

Reference
Name:
Unnamed
Type:
Constituent

Results and discussion

Water solubility
Water solubility:
> 700 g/L
Temp.:
20 °C
pH:
10.8
Details on results:
Preliminary tests:
IIn a preliminary test the test substance was easily soluble in water. As a consequence of this result the flask method was applied for the final test.

Results:
As mentioned above , the solubility of “D-VAL-DANE” in distilled water 20°C could not be determinate because the solution got such a high viscosity that further handling of the solution was not possible.
The following concentrations were measured in the filtered solution: 756,829,989,1132,1052,688 and 776g/l. The high scattering of the values is due to the difficulties of pipetting sich high viscous solution.
The pH of the solution was 10.8 at 20°C.

At 30°C the same results were obtained. Again concentrations of more than 700 g/l were found, but a saturation was not obtained.

Conclusion:
The saturation mass concentration of “D-VAL-DANE” in distilled water at 20°C was higher than 700 g/l

Applicant's summary and conclusion

Conclusions:
Interpretation of results (migrated information): very soluble (> 10000 mg/L)
The saturation mass concentration of “D-VAL-DANE” in distilled water at 20°C was higher than 700 g/l