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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
August 1985 to October 1985
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: The test was not conducted to GLP but was conducted by a recognised accredited laboratory to a recognised method and study report is available.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
1985
Report date:
1985

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
84/449/EEC
Deviations:
no
GLP compliance:
no
Type of method:
capillary method
Remarks:
Gallenkamp MFB-595

Test material

Constituent 1
Chemical structure
Reference substance name:
Bis(3,5-bis(1,1-dimethylethyl)-2-hydroxybenzoato-O1,O2)zinc
EC Number:
403-360-0
EC Name:
Bis(3,5-bis(1,1-dimethylethyl)-2-hydroxybenzoato-O1,O2)zinc
Cas Number:
42405-40-3
Molecular formula:
C30H42O6Zn
IUPAC Name:
bis(3,5-bis(1,1-dimethylethyl)-2-hydroxybenzoato-O1,O2)zinc
Details on test material:

- Physical state: solid
- Impurities (identity and concentrations): Water content was measured by Karl Fischer titration and determined to be 2.2+/-0.1%
- Purity test date: Not stated
- Lot/batch No.: Not stated
- Expiration date of the lot/batch: Not stated
- Stability under test conditions: Not stated
- Storage condition of test material: Not stated
- Other:

Results and discussion

Melting / freezing point
Melting / freezing pt.:
>= 515 - <= 517.2 K
Remarks on result:
other: Conducted at atmospheric pressure

Any other information on results incl. tables

Melting was observed to start at 515.7K and the final melting temperature was 517.2K.

Applicant's summary and conclusion

Conclusions:
Based on testing using the capillary method at standard atmospheric pressure, the melting point of the substance is 515.7 to 517.2K.
Executive summary:

The study was conducted by a recognised GLP accredited laboratory, although the study report makes no claim of GLP compliance. Testing was conducted in accordance with method A1 of EEC Directove 84/449/EEC and determined the melting point at atmospheric pressure is in the range 515 to 517.2K.