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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
07 March 2016 to 20 July 2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2016
Report date:
2016

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
Lanolin, hydroxylated
EC Number:
270-315-8
EC Name:
Lanolin, hydroxylated
Cas Number:
68424-66-8
IUPAC Name:
Lanolin, hydroxylated
Test material form:
solid

Results and discussion

Boiling point
Key result
Atm. press.:
101 kPa
Decomposition:
yes
Decomp. temp.:
155 °C

Any other information on results incl. tables

Thermographic Data

Temperature (°C)

Thermal Event

Interpretation

Determination 1

Determination 2

Exotherm

Approximate onset of decomposition

154.66

160.83

Atmospheric pressure: 101 kPa

After heating to 400 °C, the samples had lost approximately 64% of their original weight.

Overall result: decomposition from approximately 155 °C (428 K)

As a result of the low rate of enthalpy change during decomposition, the onset temperature could only be approximated. Two further thermograms were run for additional information. These showed that after being heated to 150 °C and 300 °C they had lost none and 7% of their original weight respectively. The appearance of the residue after being heated to 150 °C was similar to that of the original test item; this also suggested that decomposition had not occurred up to 150 °C.

Applicant's summary and conclusion

Conclusions:
The test item has been determined to decompose from approximately 155 °C (428 K) at 101 kPa. As the test item decomposed, no value for boiling temperature could be determined.
Executive summary:

Decomposition from approximately 155 °C (428 K) at 101 kPa by differential scanning calorimetry, designed to be compatible with Method A.2 Boiling Temperature of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 103 of the OECD Guidelines for Testing of Chemicals, 27 July 1995. As the test item decomposed, no value for boiling temperature could be determined.