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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

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Diss Factsheets

Administrative data

Endpoint:
auto-ignition temperature (liquids)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
06 January to 03 February 2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2016
Report date:
2016

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.15 (Auto-Ignition Temperature (Liquids and Gases))
Qualifier:
according to guideline
Guideline:
DIN 51794 (Testing of mineral oil hydrocarbons - Determination of ignition temperature)
GLP compliance:
no

Test material

Constituent 1
Chemical structure
Reference substance name:
rel-(1R,6S)-ethyl 2-methyl-4-oxo-6-pentylcyclohex-2-enecarboxylate
Molecular formula:
C15H24O3
IUPAC Name:
rel-(1R,6S)-ethyl 2-methyl-4-oxo-6-pentylcyclohex-2-enecarboxylate
Constituent 2
Chemical structure
Reference substance name:
rel-(1R,6R)-ethyl 2-methyl-4-oxo-6-pentylcyclohex-2-enecarboxylate
Molecular formula:
C15H24O3
IUPAC Name:
rel-(1R,6R)-ethyl 2-methyl-4-oxo-6-pentylcyclohex-2-enecarboxylate
Specific details on test material used for the study:
SOURCE OF TEST MATERIAL
- Name of test material (as stated in the report): Calyxol
- Batch No. VE00412958
- Expiration date of the lot/batch: 15.11.2017

Results and discussion

Auto-ignition temperature (liquids / gases)
Key result
Auto-ignition temperature:
375 °C
Atm. press.:
1 013 hPa

Applicant's summary and conclusion

Conclusions:
The lowest temparture giving a positive effect was 379°C. The injected volume was 100 microL, the ignition delay was 3s. At a temperature of 374°C no ignition was observed.
Therefore, after rounding off to the next lower multiple of 5°C: Auto-ignition of Calyxol: 375 +/- 10°C.
Executive summary:

The auto-ignition temperature of Calyxol was determined in a SUR BERLIN oven, equipped with a 250 mL glass ignition vessel according to the DIN 51794.

The lowest temparture giving a positive effect was 379°C. The injected volume was 100 microL, the ignition delay was 3s. At a temperature of 374°C no ignition was observed. Therefore, after rounding off to the next lower multiple of 5°C: Auto-ignition of Calyxol: 375 +/- 10°C.