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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
9 September 1996
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: GLP study conducted in accordance with OECD Guideline.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
1996
Report date:
1996

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Deviations:
no
GLP compliance:
yes
Type of method:
dynamic method

Test material

Constituent 1
Chemical structure
Reference substance name:
N1-(5-methylhexan-2-yl)benzene-1,4-diamine
Cas Number:
63302-43-2
Molecular formula:
C13H22N2
IUPAC Name:
N1-(5-methylhexan-2-yl)benzene-1,4-diamine
Details on test material:
Distilled TRAE, AA4525, lot # Y-775
Active component: 1,4-Benzenediamine, N-(1,4-dimethylpentyl)
CAS No.: 63302-43-2

Results and discussion

Boiling point
Boiling pt.:
> 300 °C
Atm. press.:
101.325 kPa

Any other information on results incl. tables

Ambient atmospheric pressure: 99.765 Kilopascals

Boiling Point at ambient pressure: greater than 300°C

Boiling Point corrected to 101.325 Kilopascals according to OECD Test # 103: greater than 300°C

The boiling point of the test sample was determined to be greater than 300 degrees C at an atmospheric pressure of 101.325 Kilopascals.

For TRAE, even though the material boiled, it could not be made to pump itself over the upper thermometer. The possible cause of this was insufficient material in the boiling tube, but, because the thermometer immersed in the boiling liquid registered the boiling point as being well above 300°C, it was not considered necessary to add more material and continue the test.

Applicant's summary and conclusion

Conclusions:
The boiling point of the substance was determined to be > 300 degrees C.
Executive summary:

The boiling point of the substance was determined using the Dynamic or Cottrell apparatus as described in OECD Guideline 104.

The boiling point of the substance was determined to be > 300 degrees C.