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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Study Experimental Work 2013-03-26 to 2013-05-31.
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Meets the criteria for classification as reliable without restriction according to Klimisch et al (1997).

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2013
Report date:
2013

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Deviations:
no
GLP compliance:
yes
Type of method:
other: Buchi melting point Apparatus B-545

Test material

Constituent 1
Chemical structure
Reference substance name:
lithium(1+) 3-[(3,4-dicyanophenyl)sulfanyl]propane-1-sulfonate
EC Number:
700-787-7
Cas Number:
769953-18-6
Molecular formula:
C11H9N2O3S2Li
IUPAC Name:
lithium(1+) 3-[(3,4-dicyanophenyl)sulfanyl]propane-1-sulfonate
Test material form:
solid: particulate/powder
Remarks:
migrated information: powder

Results and discussion

Any other information on results incl. tables

It was observed that the test material changed colour at 230°C from white to light green and that it melted around 280°C. The solution then turned dark green at 256°C. It was not possible to see bubbles in the solution, formed from the plunged end of the capillary, as the solution became black at 260°C. No further test performed as the test item degraded at around 260°C.

Applicant's summary and conclusion

Conclusions:
The boiling point could not be determined in this study as the test material degraded at 260 C.
Executive summary:

The boiling point could not be determined in this study as the test material degraded at 260 C.